[Ru(dppe)2(CCCO2 Me)(P≡C(SiMe3))][OTf]

Base Information

Chemical Name:[Ru(dppe)2(CCCO2 Me)(P≡C(SiMe3))][OTf]
CAS No.:1612234-99-7
Molecular Formula:CF₃O₃S*C₆₀H₆₀O₂P₅RuSi
Molecular Weight:1246.23
Hs Code.:

Synonyms:[Ru(dppe)2(CCCO2 Me)(P≡C(SiMe3))][OTf]

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Chemical Property of [Ru(dppe)2(CCCO2 Me)(P≡C(SiMe3))][OTf]

Chemical Property:

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Technology Process of [Ru(dppe)2(CCCO2 Me)(P≡C(SiMe3))][OTf]

There total 3 articles about [Ru(dppe)2(CCCO2 Me)(P≡C(SiMe3))][OTf] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₅₆H₅₁O₂P₄Ru⁽¹⁺⁾*CF₃O₃S^(1-)

: 75192-38-0
((trimethylsilyl)methylidyne)phosphine

: 1612234-99-7
[Ru(dppe)2(CCCO2 Me)(P≡C(SiMe3))][OTf]

Guidance literature:: In dichloromethane; at 20 ℃; for 1h; Inert atmosphere; Schlenk technique; Glovebox;
DOI:10.1039/c4dt01108b

Reference yield:

: 1612234-96-4
[RuCl(dppe)2(C≡CCO2Me)]

: 1612234-99-7
[Ru(dppe)2(CCCO2 Me)(P≡C(SiMe3))][OTf]

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 0.17 h / 20 °C / Inert atmosphere; Schlenk technique; Glovebox

2: dichloromethane / 1 h / 20 °C / Inert atmosphere; Schlenk technique; Glovebox

In dichloromethane;
DOI:10.1039/c4dt01108b

Reference yield:

: 253687-41-1
[RuCl(dppe)2]OTf

: 1612234-99-7
[Ru(dppe)2(CCCO2 Me)(P≡C(SiMe3))][OTf]

Guidance literature:: Multi-step reaction with 3 steps

1.1: dichloromethane / 16 h / 20 °C / Inert atmosphere; Schlenk technique; Glovebox

1.2: 1 h / 20 °C / Inert atmosphere; Schlenk technique; Glovebox

2.1: dichloromethane / 0.17 h / 20 °C / Inert atmosphere; Schlenk technique; Glovebox

3.1: dichloromethane / 1 h / 20 °C / Inert atmosphere; Schlenk technique; Glovebox

In dichloromethane;
DOI:10.1039/c4dt01108b