2,5-bis<6-<5-(ethoxycarbonyl)-2-<<5-(2,2-dicyanovinyl)-3-ethyl-4-methylpyrrol-2-yl>methyl>-4-methylpyrrol-3-yl>-hexyl>-1,4-dimethoxybenzene

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Chemical Name:2,5-bis<6-<5-(ethoxycarbonyl)-2-<<5-(2,2-dicyanovinyl)-3-ethyl-4-methylpyrrol-2-yl>methyl>-4-methylpyrrol-3-yl>-hexyl>-1,4-dimethoxybenzene
CAS No.:98977-22-1
Molecular Formula:C₆₀H₇₄N₈O₆
Molecular Weight:1003.3
Hs Code.:

Synonyms:2,5-bis<6-<5-(ethoxycarbonyl)-2-<<5-(2,2-dicyanovinyl)-3-ethyl-4-methylpyrrol-2-yl>methyl>-4-methylpyrrol-3-yl>-hexyl>-1,4-dimethoxybenzene

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Chemical Property of 2,5-bis<6-<5-(ethoxycarbonyl)-2-<<5-(2,2-dicyanovinyl)-3-ethyl-4-methylpyrrol-2-yl>methyl>-4-methylpyrrol-3-yl>-hexyl>-1,4-dimethoxybenzene

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Technology Process of 2,5-bis<6-<5-(ethoxycarbonyl)-2-<<5-(2,2-dicyanovinyl)-3-ethyl-4-methylpyrrol-2-yl>methyl>-4-methylpyrrol-3-yl>-hexyl>-1,4-dimethoxybenzene

There total 18 articles about 2,5-bis<6-<5-(ethoxycarbonyl)-2-<<5-(2,2-dicyanovinyl)-3-ethyl-4-methylpyrrol-2-yl>methyl>-4-methylpyrrol-3-yl>-hexyl>-1,4-dimethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 37789-74-5
5-chloromethyl-2-(β,β-dicyanovinyl)-4-ethyl-3-methylpyrrole

: 98977-20-9
2,5-bis<6-<5-(ethoxycarbonyl)-4-methylpyrrol-3-yl>hexyl>-1,4-dimethoxybenzene

: 98977-22-1
2,5-bis<6-<5-(ethoxycarbonyl)-2-<<5-(2,2-dicyanovinyl)-3-ethyl-4-methylpyrrol-2-yl>methyl>-4-methylpyrrol-3-yl>-hexyl>-1,4-dimethoxybenzene

Guidance literature:: In acetic acid; at 80 ℃;

Reference yield:

: 98990-28-4
C₃₆H₄₈N₂O₆

: 98977-22-1
2,5-bis<6-<5-(ethoxycarbonyl)-2-<<5-(2,2-dicyanovinyl)-3-ethyl-4-methylpyrrol-2-yl>methyl>-4-methylpyrrol-3-yl>-hexyl>-1,4-dimethoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1: cyclohexene / 10percent Pd/C / ethanol / 6.5 h / Heating

2: 85.4 percent / glacial acetic acid / 1 h / 80 °C

With acetic acid; cyclohexene; palladium on activated charcoal; In ethanol;
DOI:10.1021/jo00233a011

Reference yield:

: 51829-43-7
1,4-dihydroxymethyl-2,5-dimethoxybenzaldehyde

: 98977-22-1
2,5-bis<6-<5-(ethoxycarbonyl)-2-<<5-(2,2-dicyanovinyl)-3-ethyl-4-methylpyrrol-2-yl>methyl>-4-methylpyrrol-3-yl>-hexyl>-1,4-dimethoxybenzene

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) DMSO/(COCl)2, 2.)Et₃N / 1.) methylene chloride, -78 deg C, 15 min, 2.) methylene chloride, from -78 deg C to RT

2: K₂CO₃ / dioxane / Heating

3: cyclohexene / 10percent Pd/C / ethanol / 6.5 h / Heating

4: 85.4 percent / glacial acetic acid / 1 h / 80 °C

With oxalyl dichloride; potassium carbonate; acetic acid; dimethyl sulfoxide; triethylamine; cyclohexene; palladium on activated charcoal; In 1,4-dioxane; ethanol;
DOI:10.1021/jo00233a011