N-3,4-dimethoxyphenethyl-N-methyl-1-(3,4-dimethoxy-1-methylbenzocyclobutenyl)carboxamide

Base Information

Chemical Name:N-3,4-dimethoxyphenethyl-N-methyl-1-(3,4-dimethoxy-1-methylbenzocyclobutenyl)carboxamide
CAS No.:101926-88-9
Molecular Formula:C₂₃H₂₉NO₅
Molecular Weight:399.487
Hs Code.:

Synonyms:N-3,4-dimethoxyphenethyl-N-methyl-1-(3,4-dimethoxy-1-methylbenzocyclobutenyl)carboxamide

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Chemical Property of N-3,4-dimethoxyphenethyl-N-methyl-1-(3,4-dimethoxy-1-methylbenzocyclobutenyl)carboxamide

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Technology Process of N-3,4-dimethoxyphenethyl-N-methyl-1-(3,4-dimethoxy-1-methylbenzocyclobutenyl)carboxamide

There total 6 articles about N-3,4-dimethoxyphenethyl-N-methyl-1-(3,4-dimethoxy-1-methylbenzocyclobutenyl)carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 3490-06-0
N-methylhomoveratrylamine

: 101926-87-8
2,3-Dimethoxy-7-methyl-bicyclo[4.2.0]octa-1⁽⁶⁾,2,4-triene-7-carbonyl chloride

: 101926-88-9
N-3,4-dimethoxyphenethyl-N-methyl-1-(3,4-dimethoxy-1-methylbenzocyclobutenyl)carboxamide

Guidance literature:: With sodium hydrogencarbonate; In diethyl ether; water; for 2h; 0 deg C -> r.t.;
DOI:10.1039/P19850002151

Reference yield:

: 43014-33-1
3-(2,3-dimethoxyphenyl)propanenitrile

: 101926-88-9
N-3,4-dimethoxyphenethyl-N-methyl-1-(3,4-dimethoxy-1-methylbenzocyclobutenyl)carboxamide

Guidance literature:: Multi-step reaction with 6 steps

1: 65 percent / Na acetate, Br₂ / acetic acid / Ambient temperature

2: 62 percent / NaNH₂, NH₄Cl / tetrahydrofuran / 2 h / Ambient temperature

3: 98.5 percent / NaH / dimethylformamide / 2 h / 40 °C

4: 70 percent / KOH, H₂O / ethanol / 3 h / Heating

5: oxalyl chloride / CH₂Cl₂ / 1 h / Heating

6: 100 percent / NaHCO₃ / diethyl ether; H₂O / 2 h / 0 deg C -> r.t.

With potassium hydroxide; oxalyl dichloride; water; bromine; sodium acetate; sodium hydride; sodium hydrogencarbonate; ammonium chloride; sodium amide; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; water; acetic acid; N,N-dimethyl-formamide;
DOI:10.1039/P19850002151

Reference yield:

: 101926-83-4
3,4-dimethoxy-1-methylbenzocyclobutene-1-carbonitrile

: 101926-88-9
N-3,4-dimethoxyphenethyl-N-methyl-1-(3,4-dimethoxy-1-methylbenzocyclobutenyl)carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / KOH, H₂O / ethanol / 3 h / Heating

2: oxalyl chloride / CH₂Cl₂ / 1 h / Heating

3: 100 percent / NaHCO₃ / diethyl ether; H₂O / 2 h / 0 deg C -> r.t.

With potassium hydroxide; oxalyl dichloride; water; sodium hydrogencarbonate; In diethyl ether; ethanol; dichloromethane; water;
DOI:10.1039/P19850002151