6-Acetoxy-2-acetyl-2-((Z)-2-benzenesulfonyl-1-bromomethyl-vinyl)-hexanoic acid tert-butyl ester

Base Information

Chemical Name:6-Acetoxy-2-acetyl-2-((Z)-2-benzenesulfonyl-1-bromomethyl-vinyl)-hexanoic acid tert-butyl ester
CAS No.:213205-45-9
Molecular Formula:C₂₃H₃₁BrO₇S
Molecular Weight:531.465
Hs Code.:

Synonyms:6-Acetoxy-2-acetyl-2-((Z)-2-benzenesulfonyl-1-bromomethyl-vinyl)-hexanoic acid tert-butyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-Acetoxy-2-acetyl-2-((Z)-2-benzenesulfonyl-1-bromomethyl-vinyl)-hexanoic acid tert-butyl ester

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Technology Process of 6-Acetoxy-2-acetyl-2-((Z)-2-benzenesulfonyl-1-bromomethyl-vinyl)-hexanoic acid tert-butyl ester

There total 3 articles about 6-Acetoxy-2-acetyl-2-((Z)-2-benzenesulfonyl-1-bromomethyl-vinyl)-hexanoic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 2,3-dibromo-1-(phenylsulfonyl)prop-1-ene

: 22281-73-8
6-acetoxy-2-acetylhexanoic acid tert-butyl ester

: 213205-45-9
6-Acetoxy-2-acetyl-2-((Z)-2-benzenesulfonyl-1-bromomethyl-vinyl)-hexanoic acid tert-butyl ester

Guidance literature:: With sodium hydride; In tetrahydrofuran;
DOI:10.1016/S0040-4020(98)00522-5

Reference yield:

: 1694-31-1
tert-butyl acetoacetate

: 213205-45-9
6-Acetoxy-2-acetyl-2-((Z)-2-benzenesulfonyl-1-bromomethyl-vinyl)-hexanoic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) THF, 0 deg C, 30 min, 2.) THF, room temperature, overnight

2: 92 percent / NaH / tetrahydrofuran

With sodium hydride; In tetrahydrofuran;
DOI:10.1016/S0040-4020(98)00522-5

Reference yield:

: 40596-44-9
4-iodobutyl acetate

: 213205-45-9
6-Acetoxy-2-acetyl-2-((Z)-2-benzenesulfonyl-1-bromomethyl-vinyl)-hexanoic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) THF, 0 deg C, 30 min, 2.) THF, room temperature, overnight

2: 92 percent / NaH / tetrahydrofuran

With sodium hydride; In tetrahydrofuran;
DOI:10.1016/S0040-4020(98)00522-5