5-(4-methoxyphenyl)-5,6-dihydro-4H-benzo[f][1,2,3]triazolo[1,5-a][1,4]diazepine

Base Information

Chemical Name:5-(4-methoxyphenyl)-5,6-dihydro-4H-benzo[f][1,2,3]triazolo[1,5-a][1,4]diazepine
CAS No.:1358787-33-3
Molecular Formula:C₁₇H₁₆N₄O
Molecular Weight:292.34
Hs Code.:

Synonyms:5-(4-methoxyphenyl)-5,6-dihydro-4H-benzo[f][1,2,3]triazolo[1,5-a][1,4]diazepine

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Chemical Property of 5-(4-methoxyphenyl)-5,6-dihydro-4H-benzo[f][1,2,3]triazolo[1,5-a][1,4]diazepine

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Technology Process of 5-(4-methoxyphenyl)-5,6-dihydro-4H-benzo[f][1,2,3]triazolo[1,5-a][1,4]diazepine

There total 5 articles about 5-(4-methoxyphenyl)-5,6-dihydro-4H-benzo[f][1,2,3]triazolo[1,5-a][1,4]diazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 31553-17-0
1-azido-2-(bromomethyl)benzene

: 22774-66-9
N-propargyl-p-methoxyaniline

: 1358787-33-3
5-(4-methoxyphenyl)-5,6-dihydro-4H-benzo[f][1,2,3]triazolo[1,5-a][1,4]diazepine

Guidance literature:: With copper(l) iodide; potassium carbonate; In N,N-dimethyl-formamide; at 110 ℃; for 6h;
DOI:10.1016/j.tetlet.2013.08.125

Reference yield: 48.0%

: 5,6-dihydro-4H-benzo[f][1,2,3]triazolo[1,5-a][1,4]diazepine

: 104-92-7
1-bromo-4-methoxy-benzene

: 1358787-33-3
5-(4-methoxyphenyl)-5,6-dihydro-4H-benzo[f][1,2,3]triazolo[1,5-a][1,4]diazepine

Guidance literature:: With palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate; In toluene; at 80 ℃;
DOI:10.1021/co2002087

Reference yield:

: 16714-25-3
2-azidobenzaldehyde

: 1358787-33-3
5-(4-methoxyphenyl)-5,6-dihydro-4H-benzo[f][1,2,3]triazolo[1,5-a][1,4]diazepine

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium tris(acetoxy)borohydride; acetic acid / 1,2-dichloro-ethane

1.2: 100 °C

2.1: palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate / toluene / 80 °C

With palladium diacetate; sodium tris(acetoxy)borohydride; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; acetic acid; sodium t-butanolate; In 1,2-dichloro-ethane; toluene; 1.2: Huisgen dipolar cycloaddition;
DOI:10.1021/co2002087