<(2R)-2-<(4S)-2,2-dimethyl-1,3-dioxolan-4-yl>propyl>triphenylphoshonium iodide

Base Information

Chemical Name:<(2R)-2-<(4S)-2,2-dimethyl-1,3-dioxolan-4-yl>propyl>triphenylphoshonium iodide
CAS No.:95532-16-4
Molecular Formula:C₂₆H₃₀O₂P*I
Molecular Weight:532.401
Hs Code.:

Synonyms:<(2R)-2-<(4S)-2,2-dimethyl-1,3-dioxolan-4-yl>propyl>triphenylphoshonium iodide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of <(2R)-2-<(4S)-2,2-dimethyl-1,3-dioxolan-4-yl>propyl>triphenylphoshonium iodide

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Technology Process of <(2R)-2-<(4S)-2,2-dimethyl-1,3-dioxolan-4-yl>propyl>triphenylphoshonium iodide

There total 5 articles about <(2R)-2-<(4S)-2,2-dimethyl-1,3-dioxolan-4-yl>propyl>triphenylphoshonium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 74243-92-8
(4S)-4-<(1R)-2-iodo-1methylethyl>-2,2-dimethyl-1,3-dioxolane

: 603-35-0
triphenylphosphine

: 95532-16-4
<(2R)-2-<(4S)-2,2-dimethyl-1,3-dioxolan-4-yl>propyl>triphenylphoshonium iodide

Guidance literature:: With orthoformic acid triethyl ester; In acetonitrile; at 75 ℃; for 48h;
DOI:10.1021/jo00209a017

Reference yield:

: 74213-64-2
(2S,3S)-erythro-3-methylbutane-1,2,4-triol

: 95532-16-4
<(2R)-2-<(4S)-2,2-dimethyl-1,3-dioxolan-4-yl>propyl>triphenylphoshonium iodide

Guidance literature:: Multi-step reaction with 4 steps

1: 98 percent / p-TsOH / Ambient temperature

2: 97 percent / pyridine / 5 h / 0 - 20 °C

3: 85 percent / NaI / acetone / 48 h / Ambient temperature

4: 83 percent / triethyl orthoformate / acetonitrile / 48 h / 75 °C

With pyridine; toluene-4-sulfonic acid; orthoformic acid triethyl ester; sodium iodide; In acetone; acetonitrile;
DOI:10.1021/jo00209a017

Reference yield:

: 74243-88-2
(βS,4S)-β,2,3-trimethyl-1,3-dioxolane-4-ethanol

: 95532-16-4
<(2R)-2-<(4S)-2,2-dimethyl-1,3-dioxolan-4-yl>propyl>triphenylphoshonium iodide

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / pyridine / 5 h / 0 - 20 °C

2: 85 percent / NaI / acetone / 48 h / Ambient temperature

3: 83 percent / triethyl orthoformate / acetonitrile / 48 h / 75 °C

With pyridine; orthoformic acid triethyl ester; sodium iodide; In acetone; acetonitrile;
DOI:10.1021/jo00209a017