Technology Process of C34H42O5
There total 15 articles about C34H42O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
at 45 ℃;
for 2h;
Inert atmosphere;
DOI:10.1016/j.tet.2012.01.071
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: tetrahydrofuran / 3 h / 0 °C / Inert atmosphere
1.2: Saturated solution
2.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere
3.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere
3.2: 2 h / 0 - 20 °C / Inert atmosphere
4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 45 °C / Inert atmosphere
With
tetrapropylammonium perruthennate; tetrabutyl ammonium fluoride; sodium hexamethyldisilazane; 4-methylmorpholine N-oxide;
In
tetrahydrofuran; dichloromethane;
3.2: Wittig reaction;
DOI:10.1016/j.tet.2012.01.071
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere
2.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere
2.2: 2 h / 0 - 20 °C / Inert atmosphere
3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 45 °C / Inert atmosphere
With
tetrapropylammonium perruthennate; tetrabutyl ammonium fluoride; sodium hexamethyldisilazane; 4-methylmorpholine N-oxide;
In
tetrahydrofuran; dichloromethane;
2.2: Wittig reaction;
DOI:10.1016/j.tet.2012.01.071
