(E)-4-((4-((6^A-deoxy-α-cyclodextrin-6^A-yl)carbamoyl)phenyl)diazenyl)benzoic acid

Base Information

• Chemical Name: (E)-4-((4-((6^A-deoxy-α-cyclodextrin-6^A-yl)carbamoyl)phenyl)diazenyl)benzoic acid
• CAS No.: 1257331-25-1
• Molecular Formula: C₅₀H₆₉N₃O₃₂
• Molecular Weight: 1224.1
• Mol file: 1257331-25-1.mol

Synonyms:(E)-4-((4-((6^A-deoxy-α-cyclodextrin-6^A-yl)carbamoyl)phenyl)diazenyl)benzoic acid

Chemical Property of (E)-4-((4-((6^A-deoxy-α-cyclodextrin-6^A-yl)carbamoyl)phenyl)diazenyl)benzoic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of (E)-4-((4-((6^A-deoxy-α-cyclodextrin-6^A-yl)carbamoyl)phenyl)diazenyl)benzoic acid

There total 1 articles about (E)-4-((4-((6^A-deoxy-α-cyclodextrin-6^A-yl)carbamoyl)phenyl)diazenyl)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

6-deoxy-6-amino-α-cyclodextrin (29556-37-4) + (E)-azobenzene-4,4′-dicarboxylic acid (71987-42-3) → (E)-4-((4-((6A-deoxy-α-cyclodextrin-6A-yl)carbamoyl)phenyl)diazenyl)benzoic acid (1257331-25-1)

Guidance literature:

With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;

DOI:10.1002/ejoc.201900136

Reference yield: 40.0%

4,7,10-trioxa-1,13-diaminotridecane (4246-51-9) + (E)-4-((4-((6A-deoxy-α-cyclodextrin-6A-yl)carbamoyl)phenyl)diazenyl)benzoic acid (1257331-25-1) → C60H91N5O34 (1257331-26-2)

Guidance literature:

With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; In N,N-dimethyl-formamide; for 72h;

DOI:10.1002/asia.201000169

Reference yield: 36.0%

C48H100N2O22 + (E)-4-((4-((6A-deoxy-α-cyclodextrin-6A-yl)carbamoyl)phenyl)diazenyl)benzoic acid (1257331-25-1) → C98H167N5O53

Guidance literature:

With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; In N,N-dimethyl-formamide; for 72h;

DOI:10.1002/asia.201000169

upstream raw materials:

6-deoxy-6-amino-α-cyclodextrin

(E)-azobenzene-4,4′-dicarboxylic acid

Downstream raw materials:

C₆₀H₉₁N₅O₃₄