C₂₄H₂₀F₃N₅O₃

Base Information

Chemical Name:C₂₄H₂₀F₃N₅O₃
CAS No.:1397709-14-6
Molecular Formula:C₂₄H₂₀F₃N₅O₃
Molecular Weight:483.45
Hs Code.:

C<sub>24</sub>H<sub>20</sub>F<sub>3</sub>N<sub>5</sub>O<sub>3</sub>

Synonyms:C₂₄H₂₀F₃N₅O₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₄H₂₀F₃N₅O₃

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Technology Process of C₂₄H₂₀F₃N₅O₃

There total 5 articles about C₂₄H₂₀F₃N₅O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1397709-13-5
C₃₂H₂₈F₃N₅O₄

: 1397709-14-6
C₂₄H₂₀F₃N₅O₃

Guidance literature:: With ammonium cerium (IV) nitrate; In water; acetonitrile; at 20 ℃; for 20h;
DOI:10.1002/cmdc.201200184

Reference yield:

: 5345-47-1
2-aminopyridin-3-carboxylic acid

: 1397709-14-6
C₂₄H₂₀F₃N₅O₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: 4-methyl-morpholine; isobutyl chloroformate / dichloromethane / 20 h / -20 - 20 °C

1.2: 20 h / 20 °C

1.3: 2 h / 20 °C

2.1: trifluoroacetic acid / dichloromethane

3.1: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 h / 20 °C

4.1: 2-(1H-9-azabenzotriazol-1-yl)-1,1,3,3-tetramethyluroniumhexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 h / 45 °C

5.1: ammonium cerium (IV) nitrate / water; acetonitrile / 20 h / 20 °C

With 4-methyl-morpholine; ammonium cerium (IV) nitrate; 2-(1H-9-azabenzotriazol-1-yl)-1,1,3,3-tetramethyluroniumhexafluorophosphate; sodium tris(acetoxy)borohydride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; isobutyl chloroformate; In dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/cmdc.201200184

Reference yield:

: 1397709-10-2
C₂₂H₂₆N₄O₄

: 1397709-14-6
C₂₄H₂₀F₃N₅O₃

Guidance literature:: Multi-step reaction with 4 steps

1: trifluoroacetic acid / dichloromethane

2: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 h / 20 °C

3: 2-(1H-9-azabenzotriazol-1-yl)-1,1,3,3-tetramethyluroniumhexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 h / 45 °C

4: ammonium cerium (IV) nitrate / water; acetonitrile / 20 h / 20 °C

With ammonium cerium (IV) nitrate; 2-(1H-9-azabenzotriazol-1-yl)-1,1,3,3-tetramethyluroniumhexafluorophosphate; sodium tris(acetoxy)borohydride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/cmdc.201200184