2-(2-(benzyloxy)phenoxy)-N-(2-(2,6-dimethoxyphenyl thio)ethyl)acetamide

Base Information

Chemical Name:2-(2-(benzyloxy)phenoxy)-N-(2-(2,6-dimethoxyphenyl thio)ethyl)acetamide
CAS No.:1255188-18-1
Molecular Formula:C₂₅H₂₇NO₅S
Molecular Weight:453.559
Hs Code.:

Synonyms:2-(2-(benzyloxy)phenoxy)-N-(2-(2,6-dimethoxyphenyl thio)ethyl)acetamide

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Chemical Property of 2-(2-(benzyloxy)phenoxy)-N-(2-(2,6-dimethoxyphenyl thio)ethyl)acetamide

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Technology Process of 2-(2-(benzyloxy)phenoxy)-N-(2-(2,6-dimethoxyphenyl thio)ethyl)acetamide

There total 1 articles about 2-(2-(benzyloxy)phenoxy)-N-(2-(2,6-dimethoxyphenyl thio)ethyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1255188-13-6
2-(2,6-dimethoxyphenylthio)ethanamine

: 244123-12-4
2-(2-(benzyloxy)phenoxy)acetic acid

: 1255188-18-1
2-(2-(benzyloxy)phenoxy)-N-(2-(2,6-dimethoxyphenyl thio)ethyl)acetamide

Guidance literature:: 2-(2-(benzyloxy)phenoxy)acetic acid; With chloroformic acid ethyl ester; triethylamine; In chloroform; at 0 ℃; for 0.5h;

2-(2,6-dimethoxyphenylthio)ethanamine; In chloroform; at 20 ℃; for 3h;
DOI:10.1016/j.bmc.2010.08.002

Reference yield: 52.0%

: 1255188-18-1
2-(2-(benzyloxy)phenoxy)-N-(2-(2,6-dimethoxyphenyl thio)ethyl)acetamide

: 1255187-81-5
2-(2-(benzyloxy)phenoxy)-N-(2-(2,6-dimethoxyphenylthio)ethyl)ethanamine

Guidance literature:: 2-(2-(benzyloxy)phenoxy)-N-(2-(2,6-dimethoxyphenyl thio)ethyl)acetamide; With dimethylsulfide borane complex; In tetrahydrofuran; at 20 ℃; Inert atmosphere; Reflux;

With hydrogenchloride; In tetrahydrofuran; water; at 60 ℃; for 1h;

With sodium hydroxide; In water;
DOI:10.1016/j.bmc.2010.08.002