1,1-(ethylenedioxy)-3-(10-hydroxydecyl)-4-methyl-3-(phenylsulfonyl)-cyclohexane

Base Information

Chemical Name:1,1-(ethylenedioxy)-3-(10-hydroxydecyl)-4-methyl-3-(phenylsulfonyl)-cyclohexane
CAS No.:220757-92-6
Molecular Formula:C₂₅H₄₀O₅S
Molecular Weight:452.656
Hs Code.:

Synonyms:1,1-(ethylenedioxy)-3-(10-hydroxydecyl)-4-methyl-3-(phenylsulfonyl)-cyclohexane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,1-(ethylenedioxy)-3-(10-hydroxydecyl)-4-methyl-3-(phenylsulfonyl)-cyclohexane

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Technology Process of 1,1-(ethylenedioxy)-3-(10-hydroxydecyl)-4-methyl-3-(phenylsulfonyl)-cyclohexane

There total 9 articles about 1,1-(ethylenedioxy)-3-(10-hydroxydecyl)-4-methyl-3-(phenylsulfonyl)-cyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 53463-68-6
1-bromo-10-decanol

: 220757-92-6
1,1-(ethylenedioxy)-3-(10-hydroxydecyl)-4-methyl-3-(phenylsulfonyl)-cyclohexane

Guidance literature:: 1,1-(ethylenedioxy)-4-methyl-3-(phenylsulfonyl)-cyclohexane; With n-butyllithium; triphenylmethane; In tetrahydrofuran; at -78 - 20 ℃; for 1.16667h;

1-bromo-10-decanol; With Hexamethylphosphorous triamide; In tetrahydrofuran; at -78 - -20 ℃; for 2h;

Reference yield: 97.0%

: ethyl acetate n-hexane

: 53463-68-6
1-bromo-10-decanol

: 519-73-3
triphenylmethane

: 220757-91-5
1,1-(ethylenedioxy)-4-methyl-3-(phenylsulfonyl)-cyclohexane

: 220757-92-6
1,1-(ethylenedioxy)-3-(10-hydroxydecyl)-4-methyl-3-(phenylsulfonyl)-cyclohexane

Guidance literature:: With n-butyllithium; ammonium chloride; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide;

Reference yield:

: 53463-68-6
1-bromo-10-decanol

: 220757-91-5
1,1-(ethylenedioxy)-4-methyl-3-(phenylsulfonyl)-cyclohexane

: 220757-92-6
1,1-(ethylenedioxy)-3-(10-hydroxydecyl)-4-methyl-3-(phenylsulfonyl)-cyclohexane

Guidance literature:: With n-butyllithium; Multistep reaction; 1.) THF, HMPA, -78 deg C to room temperature, 1 h, 2.) HMPT, -78 deg C to -20 deg C, 2 h;
DOI:10.1016/S0040-4020(98)00406-2