2-iodo-3,5-dimethyoxyphenyl isopropylcarbamate

Base Information

Chemical Name:2-iodo-3,5-dimethyoxyphenyl isopropylcarbamate
CAS No.:899427-52-2
Molecular Formula:C₁₂H₁₆INO₄
Molecular Weight:365.168
Hs Code.:

Synonyms:2-iodo-3,5-dimethyoxyphenyl isopropylcarbamate

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Chemical Property of 2-iodo-3,5-dimethyoxyphenyl isopropylcarbamate

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Technology Process of 2-iodo-3,5-dimethyoxyphenyl isopropylcarbamate

There total 4 articles about 2-iodo-3,5-dimethyoxyphenyl isopropylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 899427-16-8
3,5-dimethoxyphenyl isopropylcarbamate

: 899427-52-2
2-iodo-3,5-dimethyoxyphenyl isopropylcarbamate

Guidance literature:: 3,5-dimethoxyphenyl isopropylcarbamate; With N,N,N,N,-tetramethylethylenediamine; trimethylsilyl trifluoromethanesulfonate; In diethyl ether; at 0 - 25 ℃; for 0.5h;

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In diethyl ether; at -78 ℃; for 1h;

With iodine; In tetrahydrofuran; diethyl ether; at -78 ℃; for 2h; Further stages.;
DOI:10.1055/s-2007-985565

Reference yield:

: C₁₅H₂₄INO₄Si

: 899427-52-2
2-iodo-3,5-dimethyoxyphenyl isopropylcarbamate

Guidance literature:: With hydrogenchloride; In methanol; at -78 - 20 ℃;
DOI:10.1055/s-2006-926462

Reference yield:

: 500-99-2
3,5-dimethoxyphenol

: 899427-52-2
2-iodo-3,5-dimethyoxyphenyl isopropylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 97 percent / DMAP / tetrahydrofuran / Heating

2.1: TMSOTf; TMEDA / diethyl ether / 0.5 h / 0 - 25 °C

2.2: TMEDA; n-BuLi / diethyl ether / 1 h / -78 °C

2.3: I₂ / diethyl ether; tetrahydrofuran / 2 h / -78 °C

With dmap; N,N,N,N,-tetramethylethylenediamine; trimethylsilyl trifluoromethanesulfonate; In tetrahydrofuran; diethyl ether;
DOI:10.1055/s-2007-985565