Technology Process of C56H36N2
There total 4 articles about C56H36N2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium phosphate;
tris-(dibenzylideneacetone)dipalladium(0); tricyclohexylphosphine;
In
1,4-dioxane; water;
at 80 - 100 ℃;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: oxygen / 0.5 h / Reflux
2.1: potassium hexacyanoferrate(III); sodium hydroxide; water / 2 h / Cooling with ice
2.2: pH ~ 8
3.1: phosphorus pentachloride; trichlorophosphate / 8 h / Inert atmosphere; Reflux
4.1: potassium phosphate / tricyclohexylphosphine; tris-(dibenzylideneacetone)dipalladium(0) / 1,4-dioxane; water / 80 - 100 °C / Inert atmosphere
With
potassium phosphate; phosphorus pentachloride; water; oxygen; sodium hydroxide; potassium hexacyanoferrate(III); trichlorophosphate;
tris-(dibenzylideneacetone)dipalladium(0); tricyclohexylphosphine;
In
1,4-dioxane; water;
4.1: Suzuki Coupling;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: phosphorus pentachloride; trichlorophosphate / 8 h / Inert atmosphere; Reflux
2: potassium phosphate / tricyclohexylphosphine; tris-(dibenzylideneacetone)dipalladium(0) / 1,4-dioxane; water / 80 - 100 °C / Inert atmosphere
With
potassium phosphate; phosphorus pentachloride; trichlorophosphate;
tris-(dibenzylideneacetone)dipalladium(0); tricyclohexylphosphine;
In
1,4-dioxane; water;
2: Suzuki Coupling;