(77Br)bromobenzene

Base Information

Chemical Name:(77Br)bromobenzene
CAS No.:84600-74-8
Molecular Formula:C₆H₅Br
Molecular Weight:154.106
Hs Code.:

Synonyms:(77Br)bromobenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (77Br)bromobenzene

Chemical Property:

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Technology Process of (77Br)bromobenzene

There total 3 articles about (77Br)bromobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98-80-6
phenylboronic acid

: 84600-74-8
(77Br)bromobenzene

Guidance literature:: With [⁷⁷Br]bromide; tetrakis(pyridine)copper(II) bis(trifluoromethanesulfonate); In water; dimethyl sulfoxide; at 80 ℃; for 0.333333h; Inert atmosphere; Sealed tube;
DOI:10.1016/j.tetlet.2018.04.024

Reference yield:

: 79-21-0
peracetic acid

: 16759-25-4,24959-67-9
[⁷⁷Br]bromide

: 1626-00-2
phenyltrimethylgermane

: 84600-74-8
(77Br)bromobenzene

Guidance literature:: With dihydrogen peroxide; acetic acid; In acetic acid; addn. of a mixt. of solvent (0.6M MeCO2Na in MeCO2H) and oxidant (in situ generated MeCO3H from 11.4M aq H2O2 and glacial MeCO2H vol. ratio 2:1, kept at room temp. 2 h, prior to application), to dry (77)Br(1-) and Ge-compd., stirring, room temp.,30 min; quenching by transferring the vessel contens to 1M aq. NaHSO3 cooled to 0 °C, extn. with CH2Cl2, drying (CaCl2), radiochemical yield 2.4%;

Reference yield:

: 66003-76-7
Diphenyliodonium triflate

: 84600-74-8
(77Br)bromobenzene

Guidance literature:: With <77Br>bromide; aminopolyether 2.2.2; potassium carbonate; In acetonitrile; at 110 ℃; for 0.5h; other diaryliodonium salts;