C₂₉H₃₆N₈O₃*ClH

Base Information

Chemical Name:C₂₉H₃₆N₈O₃*ClH
CAS No.:1262483-67-9
Molecular Formula:C₂₉H₃₆N₈O₃*ClH
Molecular Weight:581.118
Hs Code.:

C<sub>29</sub>H<sub>36</sub>N<sub>8</sub>O<sub>3</sub>*ClH

Synonyms:C₂₉H₃₆N₈O₃*ClH

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₉H₃₆N₈O₃*ClH

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Technology Process of C₂₉H₃₆N₈O₃*ClH

There total 11 articles about C₂₉H₃₆N₈O₃*ClH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1262483-62-4
C₃₈H₅₂N₈O₅

: 1262483-67-9
C₂₉H₃₆N₈O₃*ClH

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 25 ℃; for 16h; Inert atmosphere;
DOI:10.1021/ja1071916

Reference yield:

: 80151-10-6
4-(3-hydroxy-1-propyn-1-yl)-benzaldehyde

: 1262483-67-9
C₂₉H₃₆N₈O₃*ClH

Guidance literature:: Multi-step reaction with 5 steps

1.1: 4-toluenesulfonyl azide; potassium carbonate / acetonitrile / 2 h / 25 °C / Inert atmosphere

1.2: 12 h / 25 °C / Inert atmosphere

2.1: copper(ll) sulfate pentahydrate; copper / tetrahydrofuran; water / 12 h / 25 °C / Inert atmosphere

3.1: manganese(IV) oxide; potassium hydroxide / diethyl ether / 3 h / 25 °C / Inert atmosphere

4.1: copper(ll) sulfate pentahydrate; copper / tetrahydrofuran; water / 12 h / 25 °C / Inert atmosphere

5.1: hydrogenchloride / 1,4-dioxane / 16 h / 25 °C / Inert atmosphere

With hydrogenchloride; manganese(IV) oxide; 4-toluenesulfonyl azide; copper(ll) sulfate pentahydrate; copper; potassium carbonate; potassium hydroxide; In tetrahydrofuran; 1,4-dioxane; diethyl ether; water; acetonitrile; 1.1: Ohira-Bestmann reaction / 1.2: Ohira-Bestmann reaction;
DOI:10.1021/ja1071916

Reference yield:

: 1005837-03-5
C₁₅H₂₇N₅O₃

: 1262483-67-9
C₂₉H₃₆N₈O₃*ClH

Guidance literature:: Multi-step reaction with 4 steps

1: copper(ll) sulfate pentahydrate; copper / tetrahydrofuran; water / 12 h / 25 °C / Inert atmosphere

2: manganese(IV) oxide; potassium hydroxide / diethyl ether / 3 h / 25 °C / Inert atmosphere

3: copper(ll) sulfate pentahydrate; copper / tetrahydrofuran; water / 12 h / 25 °C / Inert atmosphere

4: hydrogenchloride / 1,4-dioxane / 16 h / 25 °C / Inert atmosphere

With hydrogenchloride; manganese(IV) oxide; copper(ll) sulfate pentahydrate; copper; potassium hydroxide; In tetrahydrofuran; 1,4-dioxane; diethyl ether; water;
DOI:10.1021/ja1071916