Technology Process of C30H37F6N7O2S2*C2HF3O2
There total 8 articles about C30H37F6N7O2S2*C2HF3O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
dichloromethane;
at 20 ℃;
for 3h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h / 70 °C
1.2: 16 h / 70 °C
2.1: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane
2.2: 0.5 h
3.1: palladium 10% on activated carbon; hydrogen / ethanol / 16 h
4.1: N-ethyl-N,N-diisopropylamine / dichloromethane
5.1: dichloromethane / 3 h / 20 °C
With
palladium 10% on activated carbon; hydrogen; sodium tris(acetoxy)borohydride; potassium carbonate; N-ethyl-N,N-diisopropylamine;
In
ethanol; dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: palladium 10% on activated carbon; hydrogen / ethanol / 16 h
2: N-ethyl-N,N-diisopropylamine / dichloromethane
3: dichloromethane / 3 h / 20 °C
With
palladium 10% on activated carbon; hydrogen; N-ethyl-N,N-diisopropylamine;
In
ethanol; dichloromethane;