Technology Process of C15H22O2
There total 6 articles about C15H22O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dicarbonyl(chloro)(η5-pentaphenylcyclopentadienyl)ruthenium(II); potassium tert-butylate; sodium carbonate;
In
di-isopropyl ether;
at 30 ℃;
for 145h;
optical yield given as %ee;
enantioselective reaction;
Inert atmosphere;
Molecular sieve;
Enzymatic reaction;
DOI:10.1039/c2ob25614b
- Guidance literature:
-
With
Toyonite-200M-supported Burkholderia cepacia lipase I287F/I290A mutant;
In
di-isopropyl ether;
at 30 ℃;
for 9h;
optical yield given as %ee;
enantioselective reaction;
Molecular sieve;
Enzymatic reaction;
DOI:10.1039/c2ob25614b
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: magnesium; ethylene dibromide / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere
1.2: 3.25 h / 20 °C / Inert atmosphere; Cooling with ice
1.3: pH 4 / Inert atmosphere
2.1: dicarbonyl(chloro)(η5-pentaphenylcyclopentadienyl)ruthenium(II); potassium tert-butylate; sodium carbonate / di-isopropyl ether / 145 h / 30 °C / Inert atmosphere; Molecular sieve; Enzymatic reaction
With
dicarbonyl(chloro)(η5-pentaphenylcyclopentadienyl)ruthenium(II); potassium tert-butylate; sodium carbonate; magnesium; ethylene dibromide;
In
tetrahydrofuran; di-isopropyl ether;
DOI:10.1039/c2ob25614b
