methylene[2,2,3,3-tetrakis(triisopropylphenyl)azadigermiridin-1-yl]amine

Base Information

Chemical Name:methylene[2,2,3,3-tetrakis(triisopropylphenyl)azadigermiridin-1-yl]amine
CAS No.:240434-62-2
Molecular Formula:C₆₁H₉₄Ge₂N₂
Molecular Weight:1000.61
Hs Code.:

Synonyms:methylene[2,2,3,3-tetrakis(triisopropylphenyl)azadigermiridin-1-yl]amine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methylene[2,2,3,3-tetrakis(triisopropylphenyl)azadigermiridin-1-yl]amine

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Technology Process of methylene[2,2,3,3-tetrakis(triisopropylphenyl)azadigermiridin-1-yl]amine

There total 2 articles about methylene[2,2,3,3-tetrakis(triisopropylphenyl)azadigermiridin-1-yl]amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 115534-72-0
tetrakis(2,4,6-triisopropylphenyl)digermene

: 240434-62-2
methylene[2,2,3,3-tetrakis(triisopropylphenyl)azadigermiridin-1-yl]amine

Guidance literature:: With copper; In 1,2-dimethoxyethane; diethyl ether; Ar-atmosphere; dropwise addn. of CH2N2 (in Et2O) to suspn. of Ge-compd. and Cu (in DME) at -30°C, warming to room temp., stirring (36 h); filtration (SiO2 pad), filtrate concg., crystn. (-18°C); elem. anal.;
DOI:10.1021/om990337d

Reference yield:

: 21524-34-5
2,4,6-triisopropyl-1-bromobenzene

: 240434-62-2
methylene[2,2,3,3-tetrakis(triisopropylphenyl)azadigermiridin-1-yl]amine

Guidance literature:: Multi-step reaction with 2 steps

1: n-butyllithium / diethyl ether

2: copper / diethyl ether; 1,2-dimethoxyethane

With n-butyllithium; copper; In 1,2-dimethoxyethane; diethyl ether;
DOI:10.1021/om990337d