N-carboxy Boc-Phe-ΔLeu anhydride

Base Information

Chemical Name:N-carboxy Boc-Phe-ΔLeu anhydride
CAS No.:113378-38-4
Molecular Formula:C₂₁H₂₆N₂O₆
Molecular Weight:402.447
Hs Code.:

Synonyms:N-carboxy Boc-Phe-ΔLeu anhydride

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Chemical Property of N-carboxy Boc-Phe-ΔLeu anhydride

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Technology Process of N-carboxy Boc-Phe-ΔLeu anhydride

There total 1 articles about N-carboxy Boc-Phe-ΔLeu anhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 80465-33-4
4-isobutylidene-oxazolidine-2,5-dione

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 113378-38-4
N-carboxy Boc-Phe-ΔLeu anhydride

Guidance literature:: With pyridine; dicyclohexyl-carbodiimide; In dichloromethane; at -10 - 20 ℃; for 13h;
DOI:10.3987/R-1987-08-2087

Reference yield:

: 113378-38-4
N-carboxy Boc-Phe-ΔLeu anhydride

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / CH₂Cl₂ / 20 °C

2: 2-mercaptoethanol; McIlvaine buffer / papain (EC 3.4.22.2) / 24 h / 35 °C / pH 8.0

With McIlvaine buffer; triethylamine; 2-hydroxyethanethiol; papain (EC 3.4.22.2); In dichloromethane; 1: Condensation / 2: Hydrolysis;
DOI:10.1246/bcsj.70.1427