dodecanoic acid [4-(tert-butyl-dimethyl-silanyloxy)-2-dodecanoyl-phenyl]-amide

Base Information

Chemical Name:dodecanoic acid [4-(tert-butyl-dimethyl-silanyloxy)-2-dodecanoyl-phenyl]-amide
CAS No.:923603-49-0
Molecular Formula:C₃₆H₆₅NO₃Si
Molecular Weight:588.002
Hs Code.:

dodecanoic acid [4-(<i>tert</i>-butyl-dimethyl-silanyloxy)-2-dodecanoyl-phenyl]-amide

Synonyms:dodecanoic acid [4-(tert-butyl-dimethyl-silanyloxy)-2-dodecanoyl-phenyl]-amide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dodecanoic acid [4-(tert-butyl-dimethyl-silanyloxy)-2-dodecanoyl-phenyl]-amide

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Technology Process of dodecanoic acid [4-(tert-butyl-dimethyl-silanyloxy)-2-dodecanoyl-phenyl]-amide

There total 2 articles about dodecanoic acid [4-(tert-butyl-dimethyl-silanyloxy)-2-dodecanoyl-phenyl]-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 923603-41-2
1-(2-amino-5-(tert-butyldimethylsilyloxy)phenyl)dodecan-1-one

: 112-16-3
n-dodecanoyl chloride

: 923603-49-0
dodecanoic acid [4-(tert-butyl-dimethyl-silanyloxy)-2-dodecanoyl-phenyl]-amide

Guidance literature:: With triethylamine; In dichloromethane;
DOI:10.1021/ol062540s

Reference yield:

: dodecanoic acid [4-(tert-butyl-dimethyl-silanyloxy)-phenyl]-amide

: 923603-49-0
dodecanoic acid [4-(tert-butyl-dimethyl-silanyloxy)-2-dodecanoyl-phenyl]-amide

Guidance literature:: Multi-step reaction with 2 steps

1: 55 percent / acetonitrile / 48 h / Irradiation

2: 73 percent / triethylamine / CH₂Cl₂

With triethylamine; In dichloromethane; acetonitrile; 1: Fries rearrangement;
DOI:10.1021/ol062540s