Technology Process of C37H44ClN17
There total 9 articles about C37H44ClN17 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
triethylamine;
In
N,N-dimethyl-formamide;
at 45 ℃;
for 0.166667h;
- Guidance literature:
-
Multi-step reaction with 9 steps
1: 97 percent / Na2CO3 / acetone; H2O / 5 h / 65 °C
2: tetrahydrofuran / 24 h / Heating
3: TFA / CH2Cl2 / 0.5 h
4: Et3N / CH2Cl2 / 2 h / 40 °C
5: 92 percent / tetrahydrofuran / Heating
6: hydrogen / Pd/C / tetrahydrofuran; ethanol
7: 273 mg / NaHCO3 / acetone; H2O / 2 h / 0 °C
8: aq. HCl / dioxane / 2 h
9: 61 percent / Et3N / dimethylformamide / 0.17 h / 45 °C
With
hydrogenchloride; hydrogen; sodium hydrogencarbonate; sodium carbonate; triethylamine; trifluoroacetic acid;
palladium on activated charcoal;
In
tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetone;
- Guidance literature:
-
Multi-step reaction with 8 steps
1: tetrahydrofuran / 24 h / Heating
2: TFA / CH2Cl2 / 0.5 h
3: Et3N / CH2Cl2 / 2 h / 40 °C
4: 92 percent / tetrahydrofuran / Heating
5: hydrogen / Pd/C / tetrahydrofuran; ethanol
6: 273 mg / NaHCO3 / acetone; H2O / 2 h / 0 °C
7: aq. HCl / dioxane / 2 h
8: 61 percent / Et3N / dimethylformamide / 0.17 h / 45 °C
With
hydrogenchloride; hydrogen; sodium hydrogencarbonate; triethylamine; trifluoroacetic acid;
palladium on activated charcoal;
In
tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetone;