DL-ASPARTIC-2,3,3-D3 ACID

Base Information

• Chemical Name: DL-ASPARTIC-2,3,3-D3 ACID
• CAS No.: 14341-75-4
• Molecular Formula: C₄H₇NO₄
• Molecular Weight: 136.08
• Mol file: 14341-75-4.mol

Synonyms:Aspartic-2,3,3-d3acid, DL- (8CI); DL-Aspartic-2,3,3-d3 acid

Chemical Property of DL-ASPARTIC-2,3,3-D3 ACID

Chemical Property:

• Melting Point: >300 °C (dec.)(lit.)
• PSA: 100.62000
• LogP: -0.42670
• Storage Temp.: Room Temperature
• Solubility.: Methanol (Slightly), Water (Slightly, Heated)

Purity/Quality:

99%, ^*data from raw suppliers

DL-AsparticAcid-2,3,3-d3 ^*data from reagent suppliers

Safty Information:

• Safety Statements: 22-24/25

MSDS Files:

SDS file from LookChem

Useful:

• Uses: DL-Aspartic-2,3,3-d3 Acid is an intermediate in the synthesis of D-Aspartic-2,3,3-d3 Acid (A790019) which is derived from D-Asparatic Acid (A790020), which is a non-essential amino acid found in food sources. Its conjugate base D-aspartate has potential use as an therapeutic agent in the treatment of schizophrenia-related symptoms.

Technology Process of DL-ASPARTIC-2,3,3-D3 ACID

There total 3 articles about DL-ASPARTIC-2,3,3-D3 ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

aspartic Acid (617-45-8,25608-40-6,27881-03-4,32505-46-7,52526-39-3) → DL-<4-(13)C,2,3,3-(2)H3>aspartic acid (14341-75-4)

Guidance literature:

With sodium hydroxide; aluminum(III) sulfate; water-d2; pyridoxal hydrochloride; triethylamine; at 50 ℃; for 48h;

DOI:10.1021/jo00071a029

Reference yield:

sodium [13C]cyanide (57991-39-6) + (2-Acetylamino-2,2-bis-ethoxycarbonyl-ethyl)-diethyl-methyl-ammonium; iodide (144923-36-4) → DL-<4-(13)C,2,3,3-(2)H3>aspartic acid (14341-75-4)

Guidance literature:

With diclazuril; Yield given. Multistep reaction; 1) H₂O, reflux, 12 h, 2) D₂O, reflux, 18 h;

Reference yield:

→ DL-<4-(13)C,2,3,3-(2)H3>aspartic acid (14341-75-4)

Guidance literature:

DL-Asparginsaeure, Salicylaldehyd, D2O, CuSO4;

upstream raw materials:

aspartic Acid

sodium [13C]cyanide

(2-Acetylamino-2,2-bis-ethoxycarbonyl-ethyl)-diethyl-methyl-ammonium; iodide

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