C₁₁⁽¹³⁾CH₁₄O₄

Base Information

Chemical Name:C₁₁⁽¹³⁾CH₁₄O₄
CAS No.:217481-36-2
Molecular Formula:C₁₂H₁₄O₄
Molecular Weight:223.23
Hs Code.:

C<sub>11</sub><sup>(13)</sup>CH<sub>14</sub>O<sub>4</sub>

Synonyms:C₁₁⁽¹³⁾CH₁₄O₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₁⁽¹³⁾CH₁₄O₄

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Technology Process of C₁₁⁽¹³⁾CH₁₄O₄

There total 3 articles about C₁₁⁽¹³⁾CH₁₄O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₈⁽¹³⁾CH₂₀O₃

: 217481-36-2
C₁₁⁽¹³⁾CH₁₄O₄

Guidance literature:: With ozone; triethylamine;
DOI:10.1016/S0960-894X(98)00525-3

Reference yield:

: C₁₆⁽¹³⁾CH₁₆O₂

: 217481-36-2
C₁₁⁽¹³⁾CH₁₄O₄

Guidance literature:: Multi-step reaction with 2 steps

1.1: 100 percent / TsOH / ethane-1,2-diol; benzene / 4.5 h / Heating

2.1: O₃ / CH₂Cl₂ / -78 °C

2.2: Et₃N / CH₂Cl₂ / 1 h / 20 °C

With toluene-4-sulfonic acid; ozone; In dichloromethane; ethylene glycol; benzene; 1.1: acetal formation / 2.1: Oxidation / 2.2: Substitution;
DOI:10.1016/S0040-4020(00)00163-0

Reference yield:

: C₁₆⁽¹³⁾CH₁₇BrO₂

: 217481-36-2
C₁₁⁽¹³⁾CH₁₄O₄

Guidance literature:: Multi-step reaction with 3 steps

1.1: 80 percent / Ag₂CO₃ / CH₂Cl₂ / 20 °C

2.1: 100 percent / TsOH / ethane-1,2-diol; benzene / 4.5 h / Heating

3.1: O₃ / CH₂Cl₂ / -78 °C

3.2: Et₃N / CH₂Cl₂ / 1 h / 20 °C

With toluene-4-sulfonic acid; ozone; silver carbonate; In dichloromethane; ethylene glycol; benzene; 1.1: Rearrangement / 2.1: acetal formation / 3.1: Oxidation / 3.2: Substitution;
DOI:10.1016/S0040-4020(00)00163-0