2-cyanoethyl 3-nitrooxypropyl 1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)pyridine-3,5-dicarboxylate

Base Information

Chemical Name:2-cyanoethyl 3-nitrooxypropyl 1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)pyridine-3,5-dicarboxylate
CAS No.:103434-70-4
Molecular Formula:C₂₁H₂₂N₄O₉
Molecular Weight:474.427
Hs Code.:

Synonyms:2-cyanoethyl 3-nitrooxypropyl 1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)pyridine-3,5-dicarboxylate

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Chemical Property of 2-cyanoethyl 3-nitrooxypropyl 1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)pyridine-3,5-dicarboxylate

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Technology Process of 2-cyanoethyl 3-nitrooxypropyl 1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)pyridine-3,5-dicarboxylate

There total 1 articles about 2-cyanoethyl 3-nitrooxypropyl 1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)pyridine-3,5-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 99-61-6
3-nitro-benzaldehyde

: 193539-61-6
(Z)-3-Amino-but-2-enoic acid 2-cyano-ethyl ester

: 88488-49-7
3-nitrooxypropyl acetoacetate

: 103434-70-4
2-cyanoethyl 3-nitrooxypropyl 1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)pyridine-3,5-dicarboxylate

Guidance literature:: In isopropyl alcohol; for 3h; Heating;

Reference yield: 93.0%

: 103434-70-4
2-cyanoethyl 3-nitrooxypropyl 1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)pyridine-3,5-dicarboxylate

: 103434-76-0
(+/-)-1,4-dihydro-2,6-dimethyl-5-<(3-nitrooxypropoxy)carbonyl>-4-(3-nitrophenyl)pyridine-3-carboxylic acid

Guidance literature:: With sodium hydroxide; In acetone; for 2h; Ambient temperature;

Reference yield:

: 103434-70-4
2-cyanoethyl 3-nitrooxypropyl 1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)pyridine-3,5-dicarboxylate

: methyl 3-nitrooxypropyl (4S)-1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)pyridine-3,5-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 5 M NaOH / acetone / 2 h / Ambient temperature

2: 1) Ac₂O, 2) AcCl / 1) CH₂Cl₂, r.t., 5 h, 2) CH₂Cl₂, r.t., 6 h

With sodium hydroxide; acetic anhydride; acetyl chloride; In acetone;