N-(2,4-dichlorophenyl)-N'-[2-(2-trimethylsilylethynyl)phenyl]carbodiimide

Base Information

Chemical Name:N-(2,4-dichlorophenyl)-N'-[2-(2-trimethylsilylethynyl)phenyl]carbodiimide
CAS No.:450380-99-1
Molecular Formula:C₁₈H₁₆Cl₂N₂Si
Molecular Weight:359.33
Hs Code.:

Synonyms:N-(2,4-dichlorophenyl)-N'-[2-(2-trimethylsilylethynyl)phenyl]carbodiimide

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Chemical Property of N-(2,4-dichlorophenyl)-N'-[2-(2-trimethylsilylethynyl)phenyl]carbodiimide

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Technology Process of N-(2,4-dichlorophenyl)-N'-[2-(2-trimethylsilylethynyl)phenyl]carbodiimide

There total 3 articles about N-(2,4-dichlorophenyl)-N'-[2-(2-trimethylsilylethynyl)phenyl]carbodiimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 450381-19-8
N-(2,4-dichlorophenyl)-N'-[2-(2-trimethylsilylethynyl)phenyl]thiourea

: 450380-99-1
N-(2,4-dichlorophenyl)-N'-[2-(2-trimethylsilylethynyl)phenyl]carbodiimide

Guidance literature:: With dmap; methanesulfonyl chloride; triethylamine; In dichloromethane; at 20 ℃; for 0.25h;
DOI:10.1021/jm011102i

Reference yield:

: 615-43-0
2-iodophenylamine

: 450380-99-1
N-(2,4-dichlorophenyl)-N'-[2-(2-trimethylsilylethynyl)phenyl]carbodiimide

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / CuI; Et₃N / Pd(PPh₃)2Cl₂ / 18 h / 20 °C

2: 84 percent / DMAP / ethanol / 4 h / 40 °C

3: 90 percent / CH₃SO₂Cl; Et₃N; DMAP / CH₂Cl₂ / 0.25 h / 20 °C

With dmap; copper(l) iodide; methanesulfonyl chloride; triethylamine; bis-triphenylphosphine-palladium(II) chloride; In ethanol; dichloromethane; 1: Sonogashira reaction;
DOI:10.1021/jm011102i

Reference yield:

: 103529-16-4
2-[(trimethylsilyl)ethynyl]aniline

: 450380-99-1
N-(2,4-dichlorophenyl)-N'-[2-(2-trimethylsilylethynyl)phenyl]carbodiimide

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / DMAP / ethanol / 4 h / 40 °C

2: 90 percent / CH₃SO₂Cl; Et₃N; DMAP / CH₂Cl₂ / 0.25 h / 20 °C

With dmap; methanesulfonyl chloride; triethylamine; In ethanol; dichloromethane;
DOI:10.1021/jm011102i