N-[(2R,3R,4R,5S,6R)-2-Azido-6-benzyloxymethyl-4-((2R,3R,4S,5R,6R)-6-benzyloxymethyl-3,4,5-trihydroxy-tetrahydro-pyran-2-yloxy)-5-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-3-yl]-acetamide

Base Information

Chemical Name:N-[(2R,3R,4R,5S,6R)-2-Azido-6-benzyloxymethyl-4-((2R,3R,4S,5R,6R)-6-benzyloxymethyl-3,4,5-trihydroxy-tetrahydro-pyran-2-yloxy)-5-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-3-yl]-acetamide
CAS No.:290330-46-0
Molecular Formula:C₅₅H₆₄N₄O₁₄
Molecular Weight:1005.13
Hs Code.:

N-[(2R,3R,4R,5S,6R)-2-Azido-6-benzyloxymethyl-4-((2R,3R,4S,5R,6R)-6-benzyloxymethyl-3,4,5-trihydroxy-tetrahydro-pyran-2-yloxy)-5-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-3-yl]-acetamide

Synonyms:N-[(2R,3R,4R,5S,6R)-2-Azido-6-benzyloxymethyl-4-((2R,3R,4S,5R,6R)-6-benzyloxymethyl-3,4,5-trihydroxy-tetrahydro-pyran-2-yloxy)-5-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-3-yl]-acetamide

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Chemical Property of N-[(2R,3R,4R,5S,6R)-2-Azido-6-benzyloxymethyl-4-((2R,3R,4S,5R,6R)-6-benzyloxymethyl-3,4,5-trihydroxy-tetrahydro-pyran-2-yloxy)-5-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-3-yl]-acetamide

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Technology Process of N-[(2R,3R,4R,5S,6R)-2-Azido-6-benzyloxymethyl-4-((2R,3R,4S,5R,6R)-6-benzyloxymethyl-3,4,5-trihydroxy-tetrahydro-pyran-2-yloxy)-5-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-3-yl]-acetamide

There total 5 articles about N-[(2R,3R,4R,5S,6R)-2-Azido-6-benzyloxymethyl-4-((2R,3R,4S,5R,6R)-6-benzyloxymethyl-3,4,5-trihydroxy-tetrahydro-pyran-2-yloxy)-5-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-3-yl]-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 290330-43-7
Acetic acid (2R,3R,4S,5S,6R)-4,5-diacetoxy-2-[(2R,3R,4R,5S,6R)-3-acetylamino-2-azido-6-benzyloxymethyl-5-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-4-yloxy]-6-benzyloxymethyl-tetrahydro-pyran-3-yl ester

: 290330-46-0
N-[(2R,3R,4R,5S,6R)-2-Azido-6-benzyloxymethyl-4-((2R,3R,4S,5R,6R)-6-benzyloxymethyl-3,4,5-trihydroxy-tetrahydro-pyran-2-yloxy)-5-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-3-yl]-acetamide

Guidance literature:: With sodium methylate; In methanol;

Reference yield:

: 35521-01-8,168397-51-1
2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranosyl azide

: 290330-46-0
N-[(2R,3R,4R,5S,6R)-2-Azido-6-benzyloxymethyl-4-((2R,3R,4S,5R,6R)-6-benzyloxymethyl-3,4,5-trihydroxy-tetrahydro-pyran-2-yloxy)-5-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-3-yl]-acetamide

Guidance literature:: Multi-step reaction with 4 steps

1: 63 percent / Hg(CN)2; 3 Angstroem molecular sieves / CH₂Cl₂; nitromethane

2: 78 percent / NaCNBH₃; HCl; 4 Angstroem molecular sieves / diethyl ether; tetrahydrofuran

3: 93 percent / CuBr₂; Bu₄NBr; 3 Angstroem molecular sieves / CH₂Cl₂; dimethylformamide

4: 90 percent / NaOMe / methanol

With hydrogenchloride; 3 A molecular sieve; 4 A molecular sieve; tetrabutylammomium bromide; sodium methylate; mercury(II) cyanide; sodium cyanoborohydride; copper(ll) bromide; In tetrahydrofuran; methanol; diethyl ether; nitromethane; dichloromethane; N,N-dimethyl-formamide; 1: Etherification / 2: Ring cleavage / 3: Etherification / 4: Deacetylation;

Reference yield:

: 290330-34-6
2,3,4-tri-O-acetyl-6-O-benzyl-α-D-galactopyranosyl bromide

: 290330-46-0
N-[(2R,3R,4R,5S,6R)-2-Azido-6-benzyloxymethyl-4-((2R,3R,4S,5R,6R)-6-benzyloxymethyl-3,4,5-trihydroxy-tetrahydro-pyran-2-yloxy)-5-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-3-yl]-acetamide

Guidance literature:: Multi-step reaction with 4 steps

1: 63 percent / Hg(CN)2; 3 Angstroem molecular sieves / CH₂Cl₂; nitromethane

2: 78 percent / NaCNBH₃; HCl; 4 Angstroem molecular sieves / diethyl ether; tetrahydrofuran

3: 93 percent / CuBr₂; Bu₄NBr; 3 Angstroem molecular sieves / CH₂Cl₂; dimethylformamide

4: 90 percent / NaOMe / methanol

With hydrogenchloride; 3 A molecular sieve; 4 A molecular sieve; tetrabutylammomium bromide; sodium methylate; mercury(II) cyanide; sodium cyanoborohydride; copper(ll) bromide; In tetrahydrofuran; methanol; diethyl ether; nitromethane; dichloromethane; N,N-dimethyl-formamide; 1: Etherification / 2: Ring cleavage / 3: Etherification / 4: Deacetylation;