N-Boc-L-tyrosyl-D-alanyl-L-phenylalanyl-glycine pentafluorophenyl ester

Base Information

Chemical Name:N-Boc-L-tyrosyl-D-alanyl-L-phenylalanyl-glycine pentafluorophenyl ester
CAS No.:113807-19-5
Molecular Formula:C₃₄H₃₅F₅N₄O₈
Molecular Weight:722.666
Hs Code.:

Synonyms:N-Boc-L-tyrosyl-D-alanyl-L-phenylalanyl-glycine pentafluorophenyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-Boc-L-tyrosyl-D-alanyl-L-phenylalanyl-glycine pentafluorophenyl ester

Chemical Property:

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Technology Process of N-Boc-L-tyrosyl-D-alanyl-L-phenylalanyl-glycine pentafluorophenyl ester

There total 6 articles about N-Boc-L-tyrosyl-D-alanyl-L-phenylalanyl-glycine pentafluorophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 78330-94-6
N-Boc-L-tyrosyl-D-alanyl-L-phenylalanyl-glycine

: 116893-04-0
1:3 dicyclohexylcarbodiimide-pentafluorophenol complex

: 113807-19-5
N-Boc-L-tyrosyl-D-alanyl-L-phenylalanyl-glycine pentafluorophenyl ester

Guidance literature:: In tetrahydrofuran; 1 h, 0 deg C, 8 h, 20 deg C;

Reference yield:

: 30189-51-6
ethyl (N-tert-butoxycarbonyl-L-phenylalanyl)glycinate

: 113807-19-5
N-Boc-L-tyrosyl-D-alanyl-L-phenylalanyl-glycine pentafluorophenyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 88 percent / hydrogen chloride / dioxane / 0.5 h / 20 °C

2: 56 percent / triethylamine, 1-hydroxybenzotriazole, dicyclohexylcarbodiimide / dimethylformamide

3: 90 percent / 4 N hydrogen chloride / dioxane

4: 81 percent / triethylamine, 1-hydroxybenzotriazole, dicyclohexylcarbodiimide / dimethylformamide

5: 84 percent / 1 N aq. NaOH / ethanol; H₂O / 0.25 h / 20 °C

6: 94 percent / tetrahydrofuran / 1 h, 0 deg C, 8 h, 20 deg C

With hydrogenchloride; sodium hydroxide; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; 1,4-dioxane; ethanol; water; N,N-dimethyl-formamide;

Reference yield:

: 78330-92-4
N-Boc-L-tyrosyl-D-alanyl-L-phenylalanyl-glycine ethyl ester

: 113807-19-5
N-Boc-L-tyrosyl-D-alanyl-L-phenylalanyl-glycine pentafluorophenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / 1 N aq. NaOH / ethanol; H₂O / 0.25 h / 20 °C

2: 94 percent / tetrahydrofuran / 1 h, 0 deg C, 8 h, 20 deg C

With sodium hydroxide; In tetrahydrofuran; ethanol; water;