1,1-[bis-4-(sulfamoyloxyphenyl)]-2-[4-(3,3-dimethyltriazenyl-1)-phenyl]ethene

Base Information

Chemical Name:1,1-[bis-4-(sulfamoyloxyphenyl)]-2-[4-(3,3-dimethyltriazenyl-1)-phenyl]ethene
CAS No.:1399204-67-1
Molecular Formula:C₂₂H₂₃N₅O₆S₂
Molecular Weight:517.587
Hs Code.:

Synonyms:1,1-[bis-4-(sulfamoyloxyphenyl)]-2-[4-(3,3-dimethyltriazenyl-1)-phenyl]ethene

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Chemical Property of 1,1-[bis-4-(sulfamoyloxyphenyl)]-2-[4-(3,3-dimethyltriazenyl-1)-phenyl]ethene

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Technology Process of 1,1-[bis-4-(sulfamoyloxyphenyl)]-2-[4-(3,3-dimethyltriazenyl-1)-phenyl]ethene

There total 6 articles about 1,1-[bis-4-(sulfamoyloxyphenyl)]-2-[4-(3,3-dimethyltriazenyl-1)-phenyl]ethene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1399205-38-9
1,1-[bis(4-hydroxyphenyl)]-2-[4-(3,3-dimethyltriazenyl-1)phenyl]ethene

: 1399204-67-1
1,1-[bis-4-(sulfamoyloxyphenyl)]-2-[4-(3,3-dimethyltriazenyl-1)-phenyl]ethene

Guidance literature:: With sulphamoyl chloride; In N,N-dimethyl acetamide; at 0 - 20 ℃; for 3h;

Reference yield:

: triphenylphosphonium bromide

: 1399204-67-1
1,1-[bis-4-(sulfamoyloxyphenyl)]-2-[4-(3,3-dimethyltriazenyl-1)-phenyl]ethene

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / mineral oil; dimethyl sulfoxide / 1 h / Cooling with ice

1.2: 15 h / 20 °C

2.1: hydrazine hydrate / ethanol / 1 h / 50 °C / Reflux

3.1: hydrogenchloride; pyridine / water / 3 h / 150 °C

4.1: sodium nitrite; hydrogenchloride / water / 0 - 5 °C

4.2: 0.5 h

5.1: sulphamoyl chloride / N,N-dimethyl acetamide / 3 h / 0 - 20 °C

With pyridine; hydrogenchloride; sulphamoyl chloride; sodium hydride; hydrazine hydrate; sodium nitrite; In ethanol; N,N-dimethyl acetamide; water; dimethyl sulfoxide; mineral oil;

Reference yield:

: 555-16-8
4-nitrobenzaldehdye

: 1399204-67-1
1,1-[bis-4-(sulfamoyloxyphenyl)]-2-[4-(3,3-dimethyltriazenyl-1)-phenyl]ethene

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / mineral oil; dimethyl sulfoxide / 1 h / Cooling with ice

1.2: 15 h / 20 °C

2.1: hydrazine hydrate / ethanol / 1 h / 50 °C / Reflux

3.1: hydrogenchloride; pyridine / water / 3 h / 150 °C

4.1: sodium nitrite; hydrogenchloride / water / 0 - 5 °C

4.2: 0.5 h

5.1: sulphamoyl chloride / N,N-dimethyl acetamide / 3 h / 0 - 20 °C

With pyridine; hydrogenchloride; sulphamoyl chloride; sodium hydride; hydrazine hydrate; sodium nitrite; In ethanol; N,N-dimethyl acetamide; water; dimethyl sulfoxide; mineral oil;