N,N'-Bis-(3-amino-phenyl)-N'',N''-dioctyl-[1,3,5]triazine-2,4,6-triamine

Base Information

• Chemical Name: N,N'-Bis-(3-amino-phenyl)-N'',N''-dioctyl-[1,3,5]triazine-2,4,6-triamine
• CAS No.: 190138-06-8
• Molecular Formula: C₃₁H₄₈N₈
• Molecular Weight: 532.776

Synonyms:N,N'-Bis-(3-amino-phenyl)-N'',N''-dioctyl-[1,3,5]triazine-2,4,6-triamine

Chemical Property of N,N'-Bis-(3-amino-phenyl)-N'',N''-dioctyl-[1,3,5]triazine-2,4,6-triamine

Chemical Property:

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Technology Process of N,N'-Bis-(3-amino-phenyl)-N'',N''-dioctyl-[1,3,5]triazine-2,4,6-triamine

There total 2 articles about N,N'-Bis-(3-amino-phenyl)-N'',N''-dioctyl-[1,3,5]triazine-2,4,6-triamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

m-phenylenediamine (108-45-2,64554-26-3,76583-20-5) + 6-N,N-dioctylamiono-1,3,5-triazine-2,4-dichloride (117047-57-1) → N,N'-Bis-(3-amino-phenyl)-N'',N''-dioctyl-[1,3,5]triazine-2,4,6-triamine (190138-06-8)

Guidance literature:

With sodium carbonate; In 1,4-dioxane; for 5h; Heating;

DOI:10.1002/prac.19973390147

Reference yield:

n-dioctylamine (1120-48-5) → N,N'-Bis-(3-amino-phenyl)-N'',N''-dioctyl-[1,3,5]triazine-2,4,6-triamine (190138-06-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 22 percent / K₂CO₃ / acetone / 0.5 h / 0 °C

2: 74 percent / Na₂CO₃ / dioxane / 5 h / Heating

With sodium carbonate; potassium carbonate; In 1,4-dioxane; acetone;

DOI:10.1002/prac.19973390147

Reference yield: 57.0%

N,N'-Bis-(3-amino-phenyl)-N'',N''-dioctyl-[1,3,5]triazine-2,4,6-triamine (190138-06-8) + (4-chloro-phenyl)-bis-(4,6-dichloro-[1,3,5]triazin-2-yl)-amine (27315-17-9) → 11,17-Dichlor-29-dioctylamino-14-(p-chlorphenyl)-2,8,10,12,14,16,18,20,26,28,30,31,33,34-tetradecaazahexacyclo[25.3.1.13,7.19,13.115,19.121,25]pentatriaconta-1(31),3,5,7(35),9,11,13(34),15,17,19(33),21,23,25(32),27,29-pentadecaene (190138-18-2)

Guidance literature:

With potassium carbonate; In acetone; at 25 ℃; for 1.5h;

DOI:10.1002/prac.19973390147

upstream raw materials:

m-phenylenediamine

6-N,N-dioctylamiono-1,3,5-triazine-2,4-dichloride

n-dioctylamine

Downstream raw materials:

11,17-Dichlor-29-dioctylamino-14-(p-tolyl)-2,8,10,12,14,16,18,20,26,28,30,31,33,34-tetradecaazahexacyclo[25.3.1.1^3,7.1^9,13.1^15,19.1^21,25]pentatriaconta-1⁽³¹⁾,3,5,7⁽³⁵⁾,9,11,13⁽³⁴⁾,15,17,19⁽³³⁾,21,23,25⁽³²⁾,27,29-pentadecaene

11,17-Dichlor-29-dioctylamino-14-(p-chlorphenyl)-2,8,10,12,14,16,18,20,26,28,30,31,33,34-tetradecaazahexacyclo[25.3.1.1^3,7.1^9,13.1^15,19.1^21,25]pentatriaconta-1⁽³¹⁾,3,5,7⁽³⁵⁾,9,11,13⁽³⁴⁾,15,17,19⁽³³⁾,21,23,25⁽³²⁾,27,29-pentadecaene

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