2,2'-[2,2'-oxybis(ethane-2,1-diyl)bis(oxy)]bis(2,1-phenylene)diphosphonic acid

Base Information

Chemical Name:2,2'-[2,2'-oxybis(ethane-2,1-diyl)bis(oxy)]bis(2,1-phenylene)diphosphonic acid
CAS No.:124551-19-5
Molecular Formula:C₁₆H₂₀O₉P₂
Molecular Weight:418.277
Hs Code.:

Synonyms:2,2'-[2,2'-oxybis(ethane-2,1-diyl)bis(oxy)]bis(2,1-phenylene)diphosphonic acid

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Chemical Property of 2,2'-[2,2'-oxybis(ethane-2,1-diyl)bis(oxy)]bis(2,1-phenylene)diphosphonic acid

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Technology Process of 2,2'-[2,2'-oxybis(ethane-2,1-diyl)bis(oxy)]bis(2,1-phenylene)diphosphonic acid

There total 2 articles about 2,2'-[2,2'-oxybis(ethane-2,1-diyl)bis(oxy)]bis(2,1-phenylene)diphosphonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 120582-95-8
1,5-bis[2-(diethoxyphosphinyl)phenoxy]-3-oxapentane

: 124551-19-5
2,2'-[2,2'-oxybis(ethane-2,1-diyl)bis(oxy)]bis(2,1-phenylene)diphosphonic acid

Guidance literature:: 1,5-bis[2-(diethoxyphosphinyl)phenoxy]-3-oxapentane; With chloro-trimethyl-silane; sodium bromide; In acetonitrile; at 80 ℃; for 6h;

With water; In acetonitrile; at 20 ℃; for 20h;
DOI:10.1134/S0036023611080043

Reference yield:

: 124551-13-9
bisdiethylene glycol

: 124551-19-5
2,2'-[2,2'-oxybis(ethane-2,1-diyl)bis(oxy)]bis(2,1-phenylene)diphosphonic acid

Guidance literature:: With chloro-trimethyl-silane; tetrabutylammomium bromide; sodium bromide; In acetonitrile; for 5h; Yield given; Heating;