Technology Process of C31H32O5
There total 11 articles about C31H32O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C31H34O6;
With
2,4,6-trichlorobenzoyl chloride; triethylamine;
In
tetrahydrofuran;
at 20 ℃;
With
dmap;
In
tetrahydrofuran; toluene;
at 110 ℃;
DOI:10.1021/ol101753y
- Guidance literature:
-
Multi-step reaction with 5 steps
1: chromium dichloride; nickel dichloride / dimethyl sulfoxide
2: acetic acid / water / 60 °C
3: dichloro bis(acetonitrile) palladium(II) / tetrahydrofuran / 6 h / 20 °C
4: lithium hydroxide / 1,4-dioxane; water / 80 °C
5: dmap; 2,4,6-trichlorobenzoyl chloride; triethylamine / tetrahydrofuran; toluene
With
chromium dichloride; dmap; dichloro bis(acetonitrile) palladium(II); 2,4,6-trichlorobenzoyl chloride; acetic acid; triethylamine; nickel dichloride; lithium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; water; dimethyl sulfoxide; toluene;
1: Nozaki-Hiyama-Kishi coupling / 5: Yamaguchi macrolactonization;
DOI:10.1021/jo2019762
- Guidance literature:
-
Multi-step reaction with 5 steps
1: chromium dichloride; nickel dichloride / dimethyl sulfoxide
2: acetic acid / water / 60 °C
3: dichloro bis(acetonitrile) palladium(II) / tetrahydrofuran / 6 h / 20 °C
4: lithium hydroxide / 1,4-dioxane; water / 80 °C
5: dmap; 2,4,6-trichlorobenzoyl chloride; triethylamine / tetrahydrofuran; toluene
With
chromium dichloride; dmap; dichloro bis(acetonitrile) palladium(II); 2,4,6-trichlorobenzoyl chloride; acetic acid; triethylamine; nickel dichloride; lithium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; water; dimethyl sulfoxide; toluene;
1: Nozaki-Hiyama-Kishi coupling / 5: Yamaguchi macrolactonization;
DOI:10.1021/jo2019762
