1-(2-Deoxy-3,5-di-O-p-toluoyl-β-D-erythro-pentofuranosyl)-4,7-dihydropyrazolo<3,4-b>pyridin-4-one

Base Information

Chemical Name:1-(2-Deoxy-3,5-di-O-p-toluoyl-β-D-erythro-pentofuranosyl)-4,7-dihydropyrazolo<3,4-b>pyridin-4-one
CAS No.:119368-31-9
Molecular Formula:C₂₇H₂₅N₃O₆
Molecular Weight:487.512
Hs Code.:

Synonyms:1-(2-Deoxy-3,5-di-O-p-toluoyl-β-D-erythro-pentofuranosyl)-4,7-dihydropyrazolo<3,4-b>pyridin-4-one

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Chemical Property of 1-(2-Deoxy-3,5-di-O-p-toluoyl-β-D-erythro-pentofuranosyl)-4,7-dihydropyrazolo<3,4-b>pyridin-4-one

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Technology Process of 1-(2-Deoxy-3,5-di-O-p-toluoyl-β-D-erythro-pentofuranosyl)-4,7-dihydropyrazolo<3,4-b>pyridin-4-one

There total 4 articles about 1-(2-Deoxy-3,5-di-O-p-toluoyl-β-D-erythro-pentofuranosyl)-4,7-dihydropyrazolo<3,4-b>pyridin-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 119368-16-0
C₃₄H₃₁N₃O₆

: 119368-31-9
1-(2-Deoxy-3,5-di-O-p-toluoyl-β-D-erythro-pentofuranosyl)-4,7-dihydropyrazolo<3,4-b>pyridin-4-one

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; for 2h; under 2327.2 Torr; Ambient temperature;
DOI:10.1021/jm00125a004

Reference yield:

: 4330-21-6
2-deoxy-3,5-di-O-p-toluoyl-α-D-erythro-pentofuranosyl chloride

: 119368-31-9
1-(2-Deoxy-3,5-di-O-p-toluoyl-β-D-erythro-pentofuranosyl)-4,7-dihydropyrazolo<3,4-b>pyridin-4-one

Guidance literature:: Multi-step reaction with 2 steps

1: 1) NaH / 1) CH₃CN, r.t., 1 h, 2) CH₃CN, r.t., 2 h

2: H₂ / 10percent Pd/C / ethanol / 2 h / 2327.2 Torr / Ambient temperature

With hydrogen; sodium hydride; palladium on activated charcoal; In ethanol;
DOI:10.1021/jm00125a004

Reference yield:

: 29274-28-0
4-Chloro-1H-pyrazolo<3,4-b>pyridine

: 119368-31-9
1-(2-Deoxy-3,5-di-O-p-toluoyl-β-D-erythro-pentofuranosyl)-4,7-dihydropyrazolo<3,4-b>pyridin-4-one

Guidance literature:: Multi-step reaction with 3 steps

1: 55 percent / 1) Na / 2) 170 deg C, 16 h

2: 1) NaH / 1) CH₃CN, r.t., 1 h, 2) CH₃CN, r.t., 2 h

3: H₂ / 10percent Pd/C / ethanol / 2 h / 2327.2 Torr / Ambient temperature

With hydrogen; sodium; sodium hydride; palladium on activated charcoal; In ethanol;
DOI:10.1021/jm00125a004