C₃₈H₄₈O₈Si

Base Information

Chemical Name:C₃₈H₄₈O₈Si
CAS No.:1365537-51-4
Molecular Formula:C₃₈H₄₈O₈Si
Molecular Weight:660.88
Hs Code.:

C<sub>38</sub>H<sub>48</sub>O<sub>8</sub>Si

Synonyms:C₃₈H₄₈O₈Si

Suppliers and Price of C₃₈H₄₈O₈Si

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₈H₄₈O₈Si

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₈H₄₈O₈Si

There total 13 articles about C₃₈H₄₈O₈Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₈H₄₆O₆Si

: 1365537-51-4
C₃₈H₄₈O₈Si

Guidance literature:: With methanesulfonamide; AD-mix-α; In tetrahydrofuran; water; tert-butyl alcohol; at -1 ℃; for 96h; enantioselective reaction; Inert atmosphere;
DOI:10.1016/j.tetasy.2013.02.012

Reference yield:

: 1365537-25-2
4-benzyloxy-6-hydroxy-2-(methoxymethoxy)acetophenone

: 1365537-51-4
C₃₈H₄₈O₈Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 - 20 °C

1.2: 1.08 h / 0 - 20 °C

1.3: 0 °C

2.1: sodium tetrahydroborate; cerium(III) chloride heptahydrate / tetrahydrofuran; ethanol / 5.08 h / -40 - 0 °C

3.1: 1H-imidazole / N,N-dimethyl-formamide / 16 h / 20 °C

4.1: AD-mix-α; methanesulfonamide; water / tetrahydrofuran; tert-butyl alcohol / 16 h / 0 - 20 °C

With 1H-imidazole; sodium tetrahydroborate; methanesulfonamide; cerium(III) chloride heptahydrate; AD-mix-α; water; sodium hydride; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide; mineral oil; tert-butyl alcohol; 4.1: Sharpless dihydroxylation;
DOI:10.1016/j.tetlet.2012.01.054

Reference yield:

: 480-66-0,67471-34-5
2,4,6-trihydroxyacetophenone

: 1365537-51-4
C₃₈H₄₈O₈Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

1.2: 4 h / Inert atmosphere; Reflux

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.5 h / 3 °C / Inert atmosphere

3.1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 1 h / 3 °C / Inert atmosphere

4.1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 75 °C / Inert atmosphere

5.1: sodium hydride / n-heptane; N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C / Inert atmosphere

5.2: 2.17 h / 0 - 20 °C / Inert atmosphere

6.1: cerium(III) chloride heptahydrate; sodium tetrahydroborate / tetrahydrofuran; ethanol / 65 h / 2 °C / Inert atmosphere

6.2: Inert atmosphere

7.1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

8.1: AD-mix-α; methanesulfonamide / tetrahydrofuran; water; tert-butyl alcohol / 96 h / -1 °C / Inert atmosphere

With 1H-imidazole; sodium tetrahydroborate; methanesulfonamide; cerium(III) chloride heptahydrate; AD-mix-α; tetrabutyl ammonium fluoride; sodium hydride; potassium carbonate; acetic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; ethanol; n-heptane; dichloromethane; water; N,N-dimethyl-formamide; mineral oil; tert-butyl alcohol; 5.1: |Aldol Condensation / 5.2: |Aldol Condensation / 8.1: |Sharpless Dihydroxylation;
DOI:10.1016/j.tetasy.2013.02.012