methyl 3-amino-2-bromo-5-chlorobenzoate

Base Information

Chemical Name:methyl 3-amino-2-bromo-5-chlorobenzoate
CAS No.:1403596-33-7
Molecular Formula:C₈H₇BrClNO₂
Molecular Weight:264.506
Hs Code.:

Synonyms:methyl 3-amino-2-bromo-5-chlorobenzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 3-amino-2-bromo-5-chlorobenzoate

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Technology Process of methyl 3-amino-2-bromo-5-chlorobenzoate

There total 3 articles about methyl 3-amino-2-bromo-5-chlorobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1403596-31-5
methyl 2-bromo-5-chloro-3-nitrobenzoate

: 1403596-33-7
methyl 3-amino-2-bromo-5-chlorobenzoate

Guidance literature:: methyl 2-bromo-5-chloro-3-nitrobenzoate; With ammonium chloride; In methanol; water; at 20 - 70 ℃;

With water; iron; In methanol; at 70 ℃; for 3h;

Reference yield:

: 27007-53-0
methyl-2-bromo-5-chlorobenzoate

: 1403596-33-7
methyl 3-amino-2-bromo-5-chlorobenzoate

: C₈H₇BrClNO₂

Guidance literature:: methyl-2-bromo-5-chlorobenzoate; With sulfuric acid; nitric acid; at 5 ℃; for 0.916667h;

With iron; ammonium chloride; In methanol; water; at 70 ℃; for 3h; Overall yield = 1.6 g;

Reference yield:

: 27007-53-0
methyl-2-bromo-5-chlorobenzoate

: 1403596-33-7
methyl 3-amino-2-bromo-5-chlorobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: nitric acid; sulfuric acid / 2 h / 0 °C

2.1: ammonium chloride / water; methanol / 20 - 70 °C

2.2: 3 h / 70 °C

With sulfuric acid; nitric acid; ammonium chloride; In methanol; water;