methyl 6-cyclopropyl-3-phenylpicolinate

Base Information

Chemical Name:methyl 6-cyclopropyl-3-phenylpicolinate
CAS No.:1445596-33-7
Molecular Formula:C₁₅H₁₃NO₂
Molecular Weight:239.274
Hs Code.:

Synonyms:methyl 6-cyclopropyl-3-phenylpicolinate

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Chemical Property of methyl 6-cyclopropyl-3-phenylpicolinate

Chemical Property:

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Technology Process of methyl 6-cyclopropyl-3-phenylpicolinate

There total 9 articles about methyl 6-cyclopropyl-3-phenylpicolinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1445596-32-6
methyl 6-cyclopropyl-3-phenylpicolinate

: 1445596-33-7
methyl 6-cyclopropyl-3-phenylpicolinate

Guidance literature:: With water; lithium hydroxide; In methanol; at 80 ℃; for 1h;

Reference yield:

: 605-38-9
dimethyl 2,3-pyridinedicarboxylate

: 1445596-33-7
methyl 6-cyclopropyl-3-phenylpicolinate

Guidance literature:: Multi-step reaction with 9 steps

1.1: 3-chloro-benzenecarboperoxoic acid / chloroform / Reflux

2.1: trichlorophosphate / 2 h / Reflux

3.1: palladium diacetate; potassium phosphate monohydrate; tricyclohexylphosphine / water; toluene / 4 h / Inert atmosphere; Reflux

4.1: potassium hydroxide; water / methanol / 2 h / 0 - 60 °C

5.1: acetic anhydride / 2 h / 110 °C

5.2: 2 h / 20 °C

6.1: triethylamine; diphenyl phosphoryl azide; tert-butyl alcohol / toluene / 5 h / Reflux

6.2: 20 °C

7.1: hydrogenchloride; sodium nitrite / water / 1 h / 0 - 5 °C

7.2: 10 - 20 °C

8.1: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; toluene / 0.42 h / 120 °C / Microwave irradiation

9.1: water; lithium hydroxide / methanol / 1 h / 80 °C

With hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium phosphate monohydrate; diphenyl phosphoryl azide; water; palladium diacetate; acetic anhydride; potassium carbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; potassium hydroxide; lithium hydroxide; tert-butyl alcohol; sodium nitrite; trichlorophosphate; tricyclohexylphosphine; In methanol; chloroform; water; toluene;

Reference yield:

: 1445596-30-4
6-cyclopropylpyridine-2,3-dicarboxylic acid 2-methyl ester

: 1445596-33-7
methyl 6-cyclopropyl-3-phenylpicolinate

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine; diphenyl phosphoryl azide; tert-butyl alcohol / toluene / 5 h / Reflux

1.2: 20 °C

2.1: hydrogenchloride; sodium nitrite / water / 1 h / 0 - 5 °C

2.2: 10 - 20 °C

3.1: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; toluene / 0.42 h / 120 °C / Microwave irradiation

4.1: water; lithium hydroxide / methanol / 1 h / 80 °C

With hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; diphenyl phosphoryl azide; water; potassium carbonate; triethylamine; lithium hydroxide; tert-butyl alcohol; sodium nitrite; In methanol; water; toluene;