C₃₄H₂₇BF₂N₆O₁₁

Base Information

• Chemical Name: C₃₄H₂₇BF₂N₆O₁₁
• CAS No.: 1384575-84-1
• Molecular Formula: C₃₄H₂₇BF₂N₆O₁₁
• Molecular Weight: 744.43
• Mol file: 1384575-84-1.mol

Synonyms:C₃₄H₂₇BF₂N₆O₁₁

Chemical Property of C₃₄H₂₇BF₂N₆O₁₁

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₃₄H₂₇BF₂N₆O₁₁

There total 5 articles about C₃₄H₂₇BF₂N₆O₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

C20H19BF2N2O3 (1384575-81-8) + 2-(bromomethyl)-1,3-dinitrobenzene (93213-74-2) → C34H27BF2N6O11 (1384575-84-1)

Guidance literature:

With potassium carbonate; In acetone; at 20 - 80 ℃; for 1h; Inert atmosphere;

DOI:10.1021/ja212125w

Reference yield:

C34H31BF2N2O3 (1384575-77-2) → C34H27BF2N6O11 (1384575-84-1)

Guidance literature:

Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / methanol; dichloromethane / 17 h / 20 °C

2: potassium carbonate / acetone / 1 h / 20 - 80 °C / Inert atmosphere

With palladium 10% on activated carbon; hydrogen; potassium carbonate; In methanol; dichloromethane; acetone;

DOI:10.1021/ja212125w

Reference yield:

2,6-dinitrotoluene (606-20-2) → C34H27BF2N6O11 (1384575-84-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 13 h / 100 °C / Inert atmosphere

2: potassium carbonate / acetone / 1 h / 20 - 80 °C / Inert atmosphere

With 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; 2,2'-azobis(isobutyronitrile); potassium carbonate; In tetrachloromethane; acetone;

DOI:10.1021/ja212125w

upstream raw materials:

2,4-dimethyl-1H-pyrrole

C₂₂H₁₈O₄

C₃₄H₃₁BF₂N₂O₃

C₂₀H₁₉BF₂N₂O₃

Downstream raw materials:

C₂₇H₂₃BF₂N₄O₇