N-(tert-butyloxycarbonyl)-N-(3-methyl-but-2-enyl)-2,4,6-trimethylphenylamine

Base Information

Chemical Name:N-(tert-butyloxycarbonyl)-N-(3-methyl-but-2-enyl)-2,4,6-trimethylphenylamine
CAS No.:437613-71-3
Molecular Formula:C₁₉H₂₉NO₂
Molecular Weight:303.445
Hs Code.:

Synonyms:N-(tert-butyloxycarbonyl)-N-(3-methyl-but-2-enyl)-2,4,6-trimethylphenylamine

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Chemical Property of N-(tert-butyloxycarbonyl)-N-(3-methyl-but-2-enyl)-2,4,6-trimethylphenylamine

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Technology Process of N-(tert-butyloxycarbonyl)-N-(3-methyl-but-2-enyl)-2,4,6-trimethylphenylamine

There total 3 articles about N-(tert-butyloxycarbonyl)-N-(3-methyl-but-2-enyl)-2,4,6-trimethylphenylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 56700-69-7
(2,4,6-trimethyl-phenyl)-carbamic acid tert-butyl ester

: 870-63-3
prenyl bromide

: 437613-71-3
N-(tert-butyloxycarbonyl)-N-(3-methyl-but-2-enyl)-2,4,6-trimethylphenylamine

Guidance literature:: (2,4,6-trimethyl-phenyl)-carbamic acid tert-butyl ester; With potassium hydride; In N,N-dimethyl-formamide; at 0 - 22 ℃;

prenyl bromide; In N,N-dimethyl-formamide; at 22 ℃; for 1h; Further stages.;
DOI:10.1021/ja020259c

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 437613-71-3
N-(tert-butyloxycarbonyl)-N-(3-methyl-but-2-enyl)-2,4,6-trimethylphenylamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: 98 percent / tetrahydrofuran / 168 h / Heating

2.1: KH / dimethylformamide / 0 - 22 °C

2.2: 90 percent / dimethylformamide / 1 h / 22 °C

With potassium hydride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/ja020259c

Reference yield:

: 88-05-1
2,4,6-trimethylaniline

: 437613-71-3
N-(tert-butyloxycarbonyl)-N-(3-methyl-but-2-enyl)-2,4,6-trimethylphenylamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: 98 percent / tetrahydrofuran / 168 h / Heating

2.1: KH / dimethylformamide / 0 - 22 °C

2.2: 90 percent / dimethylformamide / 1 h / 22 °C

With potassium hydride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/ja020259c