4-(2-{[(1S,2R)-2-hydroxy-2-(4-hydroxyphenyl)-1-methylethyl]-tert-butyloxycarbonylamino}ethyl)phenylbromide

Base Information

Chemical Name:4-(2-{[(1S,2R)-2-hydroxy-2-(4-hydroxyphenyl)-1-methylethyl]-tert-butyloxycarbonylamino}ethyl)phenylbromide
CAS No.:643094-43-3
Molecular Formula:C₂₂H₂₈BrNO₄
Molecular Weight:450.373
Hs Code.:

Synonyms:4-(2-{[(1S,2R)-2-hydroxy-2-(4-hydroxyphenyl)-1-methylethyl]-tert-butyloxycarbonylamino}ethyl)phenylbromide

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Chemical Property of 4-(2-{[(1S,2R)-2-hydroxy-2-(4-hydroxyphenyl)-1-methylethyl]-tert-butyloxycarbonylamino}ethyl)phenylbromide

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Technology Process of 4-(2-{[(1S,2R)-2-hydroxy-2-(4-hydroxyphenyl)-1-methylethyl]-tert-butyloxycarbonylamino}ethyl)phenylbromide

There total 2 articles about 4-(2-{[(1S,2R)-2-hydroxy-2-(4-hydroxyphenyl)-1-methylethyl]-tert-butyloxycarbonylamino}ethyl)phenylbromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₇H₂₀BrNO₂

: 24424-99-5
di-tert-butyl dicarbonate

: 643094-43-3
4-(2-{[(1S,2R)-2-hydroxy-2-(4-hydroxyphenyl)-1-methylethyl]-tert-butyloxycarbonylamino}ethyl)phenylbromide

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 12h;
DOI:10.1021/jm8000345

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 159755-11-0
1-bromo-4-(1-bromoethyl)benzene

: 552-85-2,771-91-5,1926-72-3,13104-32-0,37692-93-6,52446-53-4,62928-85-2,62928-86-3,73027-12-0
4-((1R,2S)-2-amino-1-hydroxypropyl)phenol

: 643094-43-3
4-(2-{[(1S,2R)-2-hydroxy-2-(4-hydroxyphenyl)-1-methylethyl]-tert-butyloxycarbonylamino}ethyl)phenylbromide

Guidance literature:: In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

: 643094-43-3
4-(2-{[(1S,2R)-2-hydroxy-2-(4-hydroxyphenyl)-1-methylethyl]-tert-butyloxycarbonylamino}ethyl)phenylbromide

: 1016313-28-2
[3-isopropoxy-4-(methoxycarbonyl)phenyl]boronic acid

: C₃₃H₄₁NO₇

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In 1,2-dimethoxyethane; water; at 70 ℃; for 5h; Inert atmosphere;
DOI:10.1021/jm8000345