(S(S))-(+)-3-(2-methyl-1,3-dioxolan-2-yl)propylidene-p-toluenesulfinamide

Base Information

Chemical Name:(S(S))-(+)-3-(2-methyl-1,3-dioxolan-2-yl)propylidene-p-toluenesulfinamide
CAS No.:1355076-15-1
Molecular Formula:C₁₄H₁₉NO₃S
Molecular Weight:281.376
Hs Code.:

Synonyms:(S(S))-(+)-3-(2-methyl-1,3-dioxolan-2-yl)propylidene-p-toluenesulfinamide

Suppliers and Price of (S(S))-(+)-3-(2-methyl-1,3-dioxolan-2-yl)propylidene-p-toluenesulfinamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S(S))-(+)-3-(2-methyl-1,3-dioxolan-2-yl)propylidene-p-toluenesulfinamide

Chemical Property:

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Technology Process of (S(S))-(+)-3-(2-methyl-1,3-dioxolan-2-yl)propylidene-p-toluenesulfinamide

There total 2 articles about (S(S))-(+)-3-(2-methyl-1,3-dioxolan-2-yl)propylidene-p-toluenesulfinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 24108-29-0
3-(2-methyl-[1,3]dioxolan-2-yl)-propionaldehyde

: 188447-91-8
(S)-p-toluenesulfinimide

: 1355076-15-1
(S(S))-(+)-3-(2-methyl-1,3-dioxolan-2-yl)propylidene-p-toluenesulfinamide

Guidance literature:: With titanium(IV) tetraethanolate; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1021/jo202652f

Reference yield:

: 1355076-15-1
(S(S))-(+)-3-(2-methyl-1,3-dioxolan-2-yl)propylidene-p-toluenesulfinamide

Guidance literature:

Reference yield: 80.0%

: 79-20-9
acetic acid methyl ester

: 1355076-15-1
(S(S))-(+)-3-(2-methyl-1,3-dioxolan-2-yl)propylidene-p-toluenesulfinamide

: 1138339-14-6
(SS,S)-(+)-methyl-N-(p-toluenesulfinyl)-5-amino-7-(2-methyl-1,3-dioxolan-2-yl)-3-oxoheptanoate

Guidance literature:: acetic acid methyl ester; With sodium hexamethyldisilazane; In tetrahydrofuran; diethyl ether; at -78 ℃; Inert atmosphere;

(S(S))-(+)-3-(2-methyl-1,3-dioxolan-2-yl)propylidene-p-toluenesulfinamide; In tetrahydrofuran; diethyl ether; at -78 - -10 ℃; for 6h; Inert atmosphere;
DOI:10.1021/ol9002948