(1R^,3R^)-N,N'-diethyl-1,3-diphenyl-1,3-propanediamine

Base Information

Chemical Name:(1R^*,3R^*)-N,N'-diethyl-1,3-diphenyl-1,3-propanediamine
CAS No.:140868-01-5
Molecular Formula:C₁₉H₂₆N₂
Molecular Weight:282.429
Hs Code.:

(1R<sup>*</sup>,3R<sup>*</sup>)-N,N'-diethyl-1,3-diphenyl-1,3-propanediamine

Synonyms:(1R^*,3R^*)-N,N'-diethyl-1,3-diphenyl-1,3-propanediamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R^*,3R^*)-N,N'-diethyl-1,3-diphenyl-1,3-propanediamine

Chemical Property:

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Technology Process of (1R^*,3R^*)-N,N'-diethyl-1,3-diphenyl-1,3-propanediamine

There total 7 articles about (1R^*,3R^*)-N,N'-diethyl-1,3-diphenyl-1,3-propanediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 140867-99-8
(1R^*,3R^*)-N,N'-bisacetyl-1,3-diphenyl-1,3-propanediamine

: 140868-01-5
(1R^*,3R^*)-N,N'-diethyl-1,3-diphenyl-1,3-propanediamine

Guidance literature:: With lithium aluminium tetrahydride; In 1,2-dimethoxyethane; for 22h; Heating;
DOI:10.1055/s-1992-34183

Reference yield:

: 14371-10-9
(E)-3-phenylpropenal

: 140868-01-5
(1R^*,3R^*)-N,N'-diethyl-1,3-diphenyl-1,3-propanediamine

Guidance literature:: Multi-step reaction with 7 steps

1: 66 percent / H₂NNH₂*H₂O / ethanol / 3 h / Heating

2: 89 percent / tetrahydrofuran / 12 h / Ambient temperature

3: 27 percent / PhLi / diethyl ether; tetrahydrofuran; cyclohexane / 2 h / -78 °C

4: 50percent TFA / CH₂Cl₂ / 2 h / Ambient temperature

5: H₂ / Raney-Ni / acetic acid; CH₂Cl₂ / 72 h / 31160 Torr

6: 77 percent / CH₂Cl₂ / 0.5 h / Ambient temperature

7: 92 percent / LiAlH₄ / 1,2-dimethoxy-ethane / 22 h / Heating

With lithium aluminium tetrahydride; hydrogen; hydrazine hydrate; phenyllithium; trifluoroacetic acid; nickel; In tetrahydrofuran; 1,2-dimethoxyethane; diethyl ether; ethanol; dichloromethane; cyclohexane; acetic acid;
DOI:10.1055/s-1992-34183

Reference yield:

: 936-47-0
5-phenyl-4,5-dihydro-1H-pyrazole

: 140868-01-5
(1R^*,3R^*)-N,N'-diethyl-1,3-diphenyl-1,3-propanediamine

Guidance literature:: Multi-step reaction with 6 steps

1: 89 percent / tetrahydrofuran / 12 h / Ambient temperature

2: 27 percent / PhLi / diethyl ether; tetrahydrofuran; cyclohexane / 2 h / -78 °C

3: 50percent TFA / CH₂Cl₂ / 2 h / Ambient temperature

4: H₂ / Raney-Ni / acetic acid; CH₂Cl₂ / 72 h / 31160 Torr

5: 77 percent / CH₂Cl₂ / 0.5 h / Ambient temperature

6: 92 percent / LiAlH₄ / 1,2-dimethoxy-ethane / 22 h / Heating

With lithium aluminium tetrahydride; hydrogen; phenyllithium; trifluoroacetic acid; nickel; In tetrahydrofuran; 1,2-dimethoxyethane; diethyl ether; dichloromethane; cyclohexane; acetic acid;
DOI:10.1055/s-1992-34183