N,N'-(dodecan-1,12-diyl)bis[(3Z)-3-(benzyldisulfanyl)-4-(formylamino)penten-3-yl]bis[(2-oxo-4H-2λ5-benzo[1,3,2]dioxa)phosphate]

Base Information

Chemical Name:N,N'-(dodecan-1,12-diyl)bis[(3Z)-3-(benzyldisulfanyl)-4-(formylamino)penten-3-yl]bis[(2-oxo-4H-2λ5-benzo[1,3,2]dioxa)phosphate]
CAS No.:1378272-01-5
Molecular Formula:C₅₂H₆₆N₂O₁₀P₂S₄
Molecular Weight:1069.31
Hs Code.:

Synonyms:N,N'-(dodecan-1,12-diyl)bis[(3Z)-3-(benzyldisulfanyl)-4-(formylamino)penten-3-yl]bis[(2-oxo-4H-2λ5-benzo[1,3,2]dioxa)phosphate]

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Chemical Property of N,N'-(dodecan-1,12-diyl)bis[(3Z)-3-(benzyldisulfanyl)-4-(formylamino)penten-3-yl]bis[(2-oxo-4H-2λ5-benzo[1,3,2]dioxa)phosphate]

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Technology Process of N,N'-(dodecan-1,12-diyl)bis[(3Z)-3-(benzyldisulfanyl)-4-(formylamino)penten-3-yl]bis[(2-oxo-4H-2λ5-benzo[1,3,2]dioxa)phosphate]

There total 3 articles about N,N'-(dodecan-1,12-diyl)bis[(3Z)-3-(benzyldisulfanyl)-4-(formylamino)penten-3-yl]bis[(2-oxo-4H-2λ5-benzo[1,3,2]dioxa)phosphate] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: N,N'-(dodecan-1,12-diyl)bis[(1Z)-2-(benzyldisulfanyl)-4-hydroxy-1-methyl-buten-1-yl]diformamide

: 127164-51-6
2-chloro-4H-benzo[d][1,3,2]dioxaphosphinine 2-oxide

: 1378272-01-5
N,N'-(dodecan-1,12-diyl)bis[(3Z)-3-(benzyldisulfanyl)-4-(formylamino)penten-3-yl]bis[(2-oxo-4H-2λ5-benzo[1,3,2]dioxa)phosphate]

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 ℃; Inert atmosphere;
DOI:10.1021/jm3000328

Reference yield:

: albitiazolium

: 1378272-01-5
N,N'-(dodecan-1,12-diyl)bis[(3Z)-3-(benzyldisulfanyl)-4-(formylamino)penten-3-yl]bis[(2-oxo-4H-2λ5-benzo[1,3,2]dioxa)phosphate]

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / water / 0.5 h / Cooling with ice; Inert atmosphere

2: dmap; triethylamine / dichloromethane / 0 °C / Inert atmosphere

With dmap; triethylamine; sodium hydroxide; In dichloromethane; water;
DOI:10.1021/jm3000328

Reference yield:

: benzylthio sulfate sodium

: 1378272-01-5
N,N'-(dodecan-1,12-diyl)bis[(3Z)-3-(benzyldisulfanyl)-4-(formylamino)penten-3-yl]bis[(2-oxo-4H-2λ5-benzo[1,3,2]dioxa)phosphate]

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / water / 0.5 h / Cooling with ice; Inert atmosphere

2: dmap; triethylamine / dichloromethane / 0 °C / Inert atmosphere

With dmap; triethylamine; sodium hydroxide; In dichloromethane; water;
DOI:10.1021/jm3000328