tris(trimethylphosphine)(2-α,3-α':η4-o-naphthoquinodimethane)ruthenium(0)

Base Information

Chemical Name:tris(trimethylphosphine)(2-α,3-α':η4-o-naphthoquinodimethane)ruthenium(0)
CAS No.:123737-99-5
Molecular Formula:C₂₁H₃₇P₃Ru
Molecular Weight:483.516
Hs Code.:

Synonyms:tris(trimethylphosphine)(2-α,3-α':η4-o-naphthoquinodimethane)ruthenium(0)

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Chemical Property of tris(trimethylphosphine)(2-α,3-α':η4-o-naphthoquinodimethane)ruthenium(0)

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Technology Process of tris(trimethylphosphine)(2-α,3-α':η4-o-naphthoquinodimethane)ruthenium(0)

There total 1 articles about tris(trimethylphosphine)(2-α,3-α':η4-o-naphthoquinodimethane)ruthenium(0) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 2-lithiomethyl-3-methylnaphthalene*1,2-bis(dimethylamino)ethane

: 71936-64-6,83247-97-6,96615-09-7
trans-dichlorotetrakis(trimethylphosphine)ruthenium(II)

: 123737-99-5
tris(trimethylphosphine)(2-α,3-α':η4-o-naphthoquinodimethane)ruthenium(0)

: 594-09-2
trimethylphosphane

Guidance literature:: In diethyl ether; under N2, stirred for 24 h, addn. of water, stirred for 30 min; ether decanted, dried over Na2SO4, removal of ether, sublimation at 120°C (removal of naphthalene), residue dissolved in diethyl ether, filtered, cooled to -30°C, washed with light petroleum, dried in vacuo; elem. anal.;
DOI:10.1016/S0277-5387(00)80709-3