5-Methyl-1-benzoyl-1,2,2a,3-tetrahydrobenzindole

Base Information

Chemical Name:5-Methyl-1-benzoyl-1,2,2a,3-tetrahydrobenzindole
CAS No.:155997-37-8
Molecular Formula:C₁₉H₁₇NO
Molecular Weight:275.35
Hs Code.:

5-Methyl-1-benzoyl-1,2,2a,3-tetrahydrobenz<c,d>indole

Synonyms:5-Methyl-1-benzoyl-1,2,2a,3-tetrahydrobenzindole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-Methyl-1-benzoyl-1,2,2a,3-tetrahydrobenzindole

Chemical Property:

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Technology Process of 5-Methyl-1-benzoyl-1,2,2a,3-tetrahydrobenzindole

There total 2 articles about 5-Methyl-1-benzoyl-1,2,2a,3-tetrahydrobenzindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2811-66-7
1-benzoyl-5-methyl-1,2,2a,3,4,5-hexahydro-benzo[cd]indol-5-ol

: 155997-37-8
5-Methyl-1-benzoyl-1,2,2a,3-tetrahydrobenzindole

Guidance literature:: With toluene-4-sulfonic acid; In toluene; for 4h; Yield given; Heating;
DOI:10.1021/jo00087a042

Reference yield:

: 132008-45-8,51867-02-8
1-benzoyl-2,2a,3,4-tetrahydro-1H-benz[cd]indol-5-one

: 155997-37-8
5-Methyl-1-benzoyl-1,2,2a,3-tetrahydrobenzindole

Guidance literature:: Multi-step reaction with 2 steps

1: toluene; tetrahydrofuran / 1.) -78 deg C, 1 h, 2.) r.t., overnight

2: p-TsOH*H₂O / toluene / 4 h / Heating

With toluene-4-sulfonic acid; In tetrahydrofuran; toluene;
DOI:10.1021/jo00087a042

Reference yield: 84.0%

: 155997-37-8
5-Methyl-1-benzoyl-1,2,2a,3-tetrahydrobenzindole

: 5-Methyl-4,5-exo-epoxy-1-benzoyl-1,2,2a,3,4,5-hexahydrobenzindole

: 5-Methyl-4,5-endo-epoxy-1-benzoyl-1,2,2a,3,4,5-hexahydrobenzindole

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In chloroform; Yields of byproduct given; 1.) 0 deg C, 15 min, 2.) r.t., 2 h;
DOI:10.1021/jo00087a042