N-(5-dimethylaminonaphthalene-1-sulfonyl)-N'-(p-toluenesulfonyl)bis(3-aminopropyl)benzylamine

Base Information

Chemical Name:N-(5-dimethylaminonaphthalene-1-sulfonyl)-N'-(p-toluenesulfonyl)bis(3-aminopropyl)benzylamine
CAS No.:471866-83-8
Molecular Formula:C₃₂H₄₀N₄O₄S₂
Molecular Weight:608.826
Hs Code.:

Synonyms:N-(5-dimethylaminonaphthalene-1-sulfonyl)-N'-(p-toluenesulfonyl)bis(3-aminopropyl)benzylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(5-dimethylaminonaphthalene-1-sulfonyl)-N'-(p-toluenesulfonyl)bis(3-aminopropyl)benzylamine

Chemical Property:

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Technology Process of N-(5-dimethylaminonaphthalene-1-sulfonyl)-N'-(p-toluenesulfonyl)bis(3-aminopropyl)benzylamine

There total 5 articles about N-(5-dimethylaminonaphthalene-1-sulfonyl)-N'-(p-toluenesulfonyl)bis(3-aminopropyl)benzylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 881693-49-8
N-(5-dimethylaminonaphthalene-1-sulfonyl)-N'-(p-toluenesulfonyl)bis(3-aminopropyl)amine

: 100-44-7
benzyl chloride

: 471866-83-8
N-(5-dimethylaminonaphthalene-1-sulfonyl)-N'-(p-toluenesulfonyl)bis(3-aminopropyl)benzylamine

Guidance literature:: With sodium carbonate; sodium iodide; In acetonitrile; for 4h; Heating;
DOI:10.1021/jm0582524

Reference yield:

: 121379-43-9
3-(2-methyltetrahydropyrimidin-1-yl)propylamine

: 471866-83-8
N-(5-dimethylaminonaphthalene-1-sulfonyl)-N'-(p-toluenesulfonyl)bis(3-aminopropyl)benzylamine

Guidance literature:: Multi-step reaction with 3 steps

1: aq. NaOH / tetrahydrofuran / 20 °C

2: 50 percent / aq. Na₂CO₃ / CH₂Cl₂ / 18 h / 20 °C

3: 50 percent / Na₂CO₃; NaI / acetonitrile / 4 h / Heating

With sodium hydroxide; sodium carbonate; sodium iodide; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1021/jm0582524

Reference yield:

: 471866-81-6
3-[2-methyl-3-(p-toluenesulfonyl)tetrahydropyrimidin-1-yl]propylamine

: 471866-83-8
N-(5-dimethylaminonaphthalene-1-sulfonyl)-N'-(p-toluenesulfonyl)bis(3-aminopropyl)benzylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / aq. Na₂CO₃ / CH₂Cl₂ / 18 h / 20 °C

2: 50 percent / Na₂CO₃; NaI / acetonitrile / 4 h / Heating

With sodium carbonate; sodium iodide; In dichloromethane; acetonitrile;
DOI:10.1021/jm0582524