dimethyl 5,5'-[(2-acetyl-1,4-phenylene)bis(oxy)]bis[2,2-dimethylpentanoate]

Base Information

Chemical Name:dimethyl 5,5'-[(2-acetyl-1,4-phenylene)bis(oxy)]bis[2,2-dimethylpentanoate]
CAS No.:79520-55-1
Molecular Formula:C₂₄H₃₆O₇
Molecular Weight:436.546
Hs Code.:

Synonyms:dimethyl 5,5'-[(2-acetyl-1,4-phenylene)bis(oxy)]bis[2,2-dimethylpentanoate]

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Chemical Property of dimethyl 5,5'-[(2-acetyl-1,4-phenylene)bis(oxy)]bis[2,2-dimethylpentanoate]

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Technology Process of dimethyl 5,5'-[(2-acetyl-1,4-phenylene)bis(oxy)]bis[2,2-dimethylpentanoate]

There total 1 articles about dimethyl 5,5'-[(2-acetyl-1,4-phenylene)bis(oxy)]bis[2,2-dimethylpentanoate] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 79520-52-8
5-Bromo-2,2-dimethylpentanoic acid,methyl ester

: 490-78-8
2,5-Dihydroxyacetophenone

: 79520-55-1
dimethyl 5,5'-[(2-acetyl-1,4-phenylene)bis(oxy)]bis[2,2-dimethylpentanoate]

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1.) DMF, RT, 1 h, 2.) DMF, 80 - 85 deg C, 12 - 14 h;
DOI:10.1021/jm00361a015

Reference yield:

: 79520-55-1
dimethyl 5,5'-[(2-acetyl-1,4-phenylene)bis(oxy)]bis[2,2-dimethylpentanoate]

: 5-[2-(1-Hydroxy-ethyl)-4-(4-methoxycarbonyl-4-methyl-pentyloxy)-phenoxy]-2,2-dimethyl-pentanoic acid methyl ester

Guidance literature:: With sodium tetrahydroborate; In methanol; Ambient temperature;
DOI:10.1021/jm00361a015

Reference yield:

: 79520-55-1
dimethyl 5,5'-[(2-acetyl-1,4-phenylene)bis(oxy)]bis[2,2-dimethylpentanoate]

: 79521-05-4
5,5'-[2-(1-hydroxyethyl)-1,4-phenylenebis(oxy)]bis[2,2-dimethylpentanoic acid]

Guidance literature:: Multi-step reaction with 2 steps

1: NaBH₄ / methanol / Ambient temperature

2: 2 N NaOH / methanol

With sodium hydroxide; sodium tetrahydroborate; In methanol;
DOI:10.1021/jm00361a015