(S,E)‐4‐phenylbut‐3‐en‐2‐yl butyrate

Base Information

Chemical Name:(S,E)‐4‐phenylbut‐3‐en‐2‐yl butyrate
CAS No.:326804-18-6
Molecular Formula:C₁₄H₁₈O₂
Molecular Weight:218.296
Hs Code.:

Synonyms:(S,E)‐4‐phenylbut‐3‐en‐2‐yl butyrate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S,E)‐4‐phenylbut‐3‐en‐2‐yl butyrate

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Technology Process of (S,E)‐4‐phenylbut‐3‐en‐2‐yl butyrate

There total 5 articles about (S,E)‐4‐phenylbut‐3‐en‐2‐yl butyrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 371-27-7
2,2,2-trifluoroethylbutyrate

: 36004-04-3
ethyl (E)-1-phenylbut-1-en-3-ol

: 326804-18-6
(S,E)‐4‐phenylbut‐3‐en‐2‐yl butyrate

Guidance literature:: With chlorodicarbonyl(1-(isopropylamino)-2,3,4,5-tetraphenylcyclopentadienyl) ruthenium (II); potassium tert-butylate; sodium carbonate; In tetrahydrofuran; at 25 ℃; for 24h; enantioselective reaction; Schlenk technique; Inert atmosphere;
DOI:10.1039/c7ob02181j

Reference yield: 75.0%

: 371-27-7
2,2,2-trifluoroethylbutyrate

: 36004-04-3
ethyl (E)-1-phenylbut-1-en-3-ol

: 2550-26-7
4-Phenyl-2-butanone

: 326804-18-6
(S,E)‐4‐phenylbut‐3‐en‐2‐yl butyrate

Guidance literature:: ethyl (E)-1-phenylbut-1-en-3-ol; With dicarbonyl(chloro)(η⁵-pentaphenylcyclopentadienyl)ruthenium(II); eicosaethylene glycol hexadecyl ether; potassium tert-butylate; sodium carbonate; n-octyl β-D-glucopyranoside; subtilisin Carlsberg; In tetrahydrofuran; toluene; for 0.0666667h; Inert atmosphere; Enzymatic reaction;

2,2,2-trifluoroethylbutyrate; In tetrahydrofuran; toluene; at 40 ℃; for 48h; optical yield given as %ee; Inert atmosphere; Enzymatic reaction;
DOI:10.1021/jo1011653

Reference yield: 45.0%

: (E)‐4‐phenylbut‐3‐en‐2‐yl butyrate

: 62413-47-2
(2R,3E)-4-phenyl-3-buten-2-ol

: 326804-18-6
(S,E)‐4‐phenylbut‐3‐en‐2‐yl butyrate

Guidance literature:: With Lecitase Ultra immobilized on cyanogen bromide-activated agarose; In aq. phosphate buffer; acetone; for 24h; pH=7.2; enantioselective reaction; Resolution of racemate; Enzymatic reaction;
DOI:10.3390/molecules25051067