(5-phenyl-1,2,4-triazin-3-yl)-methanesulphonic acid 2,2-dimethyl-propyl ester

Base Information

Chemical Name:(5-phenyl-1,2,4-triazin-3-yl)-methanesulphonic acid 2,2-dimethyl-propyl ester
CAS No.:473530-13-1
Molecular Formula:C₁₅H₁₉N₃O₃S
Molecular Weight:321.4
Hs Code.:

Synonyms:(5-phenyl-1,2,4-triazin-3-yl)-methanesulphonic acid 2,2-dimethyl-propyl ester

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Chemical Property of (5-phenyl-1,2,4-triazin-3-yl)-methanesulphonic acid 2,2-dimethyl-propyl ester

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Technology Process of (5-phenyl-1,2,4-triazin-3-yl)-methanesulphonic acid 2,2-dimethyl-propyl ester

There total 1 articles about (5-phenyl-1,2,4-triazin-3-yl)-methanesulphonic acid 2,2-dimethyl-propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 18162-28-2
5-phenyl-1,2,4-triazine

: 86434-24-4
neopentyl chloromethanesulfonate

: 473530-13-1
(5-phenyl-1,2,4-triazin-3-yl)-methanesulphonic acid 2,2-dimethyl-propyl ester

Guidance literature:: With potassium hydroxide; In dimethyl sulfoxide; at 20 ℃; for 1h;
DOI:10.1248/cpb.50.463

Reference yield:

: 473530-13-1
(5-phenyl-1,2,4-triazin-3-yl)-methanesulphonic acid 2,2-dimethyl-propyl ester

: 2-phenyl-5,6,7,8-tetrahydroquinoline-8-sulphonic acid 2,2-dimethylpropyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaH / dimethylformamide / 0.25 h / 0 °C

1.2: 26 percent / dimethylformamide / 0 °C

2.1: 97 percent / various solvent(s) / 3 h / Heating

With sodium hydride; In N,N-dimethyl-formamide; 2.1: intramolecular Diels-Alder reaction;
DOI:10.1248/cpb.50.463