(2R,3S,4S)-2-(benzylamino)-4-<valyl>amino>-3-hydoxy-5-phenylpentanoic acid

Base Information

Chemical Name:(2R,3S,4S)-2-(benzylamino)-4-<valyl>amino>-3-hydoxy-5-phenylpentanoic acid
CAS No.:161510-67-4
Molecular Formula:C₃₁H₃₇N₃O₆
Molecular Weight:547.651
Hs Code.:

(2R,3S,4S)-2-(benzylamino)-4-<<N-<(benzyloxy)carbonyl>valyl>amino>-3-hydoxy-5-phenylpentanoic acid

Synonyms:(2R,3S,4S)-2-(benzylamino)-4-<valyl>amino>-3-hydoxy-5-phenylpentanoic acid

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Chemical Property of (2R,3S,4S)-2-(benzylamino)-4-<valyl>amino>-3-hydoxy-5-phenylpentanoic acid

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Technology Process of (2R,3S,4S)-2-(benzylamino)-4-<valyl>amino>-3-hydoxy-5-phenylpentanoic acid

There total 3 articles about (2R,3S,4S)-2-(benzylamino)-4-<valyl>amino>-3-hydoxy-5-phenylpentanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 161510-65-2
(2R,3S,4S)-2-(benzylamino)-4-<valyl>amino>-3-hydoxy-5-phenylpentanoic acid ethyl ester

: 161510-67-4
(2R,3S,4S)-2-(benzylamino)-4-<valyl>amino>-3-hydoxy-5-phenylpentanoic acid

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; for 10h; Ambient temperature;
DOI:10.1021/jm00045a013

Reference yield:

: (2S/R,3R,S,4S)-4-<valyl>amino>-2,3-epoxy-5-phenylpentanoic acid ethyl ester

: 161510-67-4
(2R,3S,4S)-2-(benzylamino)-4-<valyl>amino>-3-hydoxy-5-phenylpentanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / ethanol / 48 h / 60 °C

2: 89 percent / 1N aq. NaOH / tetrahydrofuran / 10 h / Ambient temperature

With sodium hydroxide; In tetrahydrofuran; ethanol;
DOI:10.1021/jm00045a013

Reference yield:

: 100-46-9
benzylamine

: 161510-67-4
(2R,3S,4S)-2-(benzylamino)-4-<valyl>amino>-3-hydoxy-5-phenylpentanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / ethanol / 48 h / 60 °C

2: 89 percent / 1N aq. NaOH / tetrahydrofuran / 10 h / Ambient temperature

With sodium hydroxide; In tetrahydrofuran; ethanol;
DOI:10.1021/jm00045a013