4-hydroxy-3-(4-hydroxymethyl-2-methoxyphenoxy)-5-methoxybenzaldehyde

Base Information

• Chemical Name: 4-hydroxy-3-(4-hydroxymethyl-2-methoxyphenoxy)-5-methoxybenzaldehyde
• CAS No.: 160097-39-2
• Molecular Formula: C₁₆H₁₆O₆
• Molecular Weight: 304.299
• Mol file: 160097-39-2.mol

Synonyms:4-hydroxy-3-(4-hydroxymethyl-2-methoxyphenoxy)-5-methoxybenzaldehyde

Chemical Property of 4-hydroxy-3-(4-hydroxymethyl-2-methoxyphenoxy)-5-methoxybenzaldehyde

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 4-hydroxy-3-(4-hydroxymethyl-2-methoxyphenoxy)-5-methoxybenzaldehyde

There total 2 articles about 4-hydroxy-3-(4-hydroxymethyl-2-methoxyphenoxy)-5-methoxybenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-hydroxymethyl-2-methoxyphenol (498-00-0) → 3-(4-formyl-2-methoxyphenoxy)-4-hydroxy-5-methoxybenzaldehyde (2555-98-8) + vanillin (121-33-5,8014-42-4) + 4-hydroxy-3-(4-hydroxymethyl-2-methoxyphenoxy)-5-methoxybenzaldehyde (160097-39-2) + C24H22O9

Guidance literature:

With silver(l) oxide; In acetone; Yield given. Yields of byproduct given;

Reference yield:

4-hydroxymethyl-2-methoxyphenol (498-00-0) → 4-hydroxy-3-(4-hydroxymethyl-2-methoxyphenoxy)-5-methoxybenzaldehyde (160097-39-2)

Guidance literature:

With silver(l) oxide; In acetone; at 20 ℃; for 0.666667h;

DOI:10.1002/chem.201201506

Reference yield: 77.0%

4-hydroxy-3-(4-hydroxymethyl-2-methoxyphenoxy)-5-methoxybenzaldehyde (160097-39-2) → 3-(4-formyl-2-methoxyphenoxy)-4-hydroxy-5-methoxybenzaldehyde (2555-98-8)

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; Ambient temperature;

upstream raw materials:

4-hydroxymethyl-2-methoxyphenol

Downstream raw materials:

3-(4-formyl-2-methoxyphenoxy)-4-hydroxy-5-methoxybenzaldehyde

4-(1-Ethoxy-ethoxy)-3-(4-formyl-2-methoxy-phenoxy)-5-methoxy-benzaldehyde

ethyl (E)-3-<4-<(E)-2-ethoxycarbonylvinyl>-2-methoxyphenoxy>-4-hydroxy-5-methoxycinnamate

C₃₆H₃₈O₁₂