3-nitro-4-trifluoromethanesulfonyloxyphenylacetic acid ethyl ester

Base Information

• Chemical Name: 3-nitro-4-trifluoromethanesulfonyloxyphenylacetic acid ethyl ester
• CAS No.: 400648-67-1
• Molecular Formula: C₁₁H₁₀F₃NO₇S
• Molecular Weight: 357.264
• Mol file: 400648-67-1.mol

Synonyms:3-nitro-4-trifluoromethanesulfonyloxyphenylacetic acid ethyl ester

Chemical Property of 3-nitro-4-trifluoromethanesulfonyloxyphenylacetic acid ethyl ester

Chemical Property:

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Technology Process of 3-nitro-4-trifluoromethanesulfonyloxyphenylacetic acid ethyl ester

There total 1 articles about 3-nitro-4-trifluoromethanesulfonyloxyphenylacetic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Ethyl 2-(4-hydroxy-3-nitrophenyl)acetate (183380-81-6) + trifluoromethanesulfonic acid anhydride (1025373-45-8) → 3-nitro-4-trifluoromethanesulfonyloxyphenylacetic acid ethyl ester (400648-67-1)

Guidance literature:

With hydrogenchloride; pyridine; In 1,2-dichloro-ethane;

Reference yield:

3-nitro-4-trifluoromethanesulfonyloxyphenylacetic acid ethyl ester (400648-67-1) + dichlorobis(triphenylphosphine)palladium[II] → 4-ethyl-3-nitrophenylacetic acid ethyl ester (400648-68-2)

Guidance literature:

With hydrogenchloride; Zinc chloride; In tetrahydrofuran; toluene;

upstream raw materials:

Ethyl 2-(4-hydroxy-3-nitrophenyl)acetate

trifluoromethanesulfonic acid anhydride

Downstream raw materials:

4-ethyl-3-nitrophenylacetic acid ethyl ester